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PROCESS FOR THE PREPARATION OF ENOL-LACTONE OF ACETIC 2-OXOCYCLOHEXYLIDENE ACID AND APPLICATION TO THE PREPARATION OF 2-COUMARANONE
PROCESS FOR THE PREPARATION OF ENOL-LACTONE OF ACETIC 2-OXOCYCLOHEXYLIDENE ACID AND APPLICATION TO THE PREPARATION OF 2-COUMARANONE
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机译:乙酸2-氧代环己烯基烯醇内酯的制备方法及其在2-香豆烷酮制备中的应用
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摘要
A process for the preparation of the enol lactone of 2-oxocyclohexylideneacetic acid in which: 1) the glyoxylic acid is reacted with cyclohexanone in the presence of a halogenated acid in order to to obtain a crude reaction B1, then BR/ 2) is reacted that reaction crude B1 after solubilization in an organic solvent in the presence of a strong acid soluble in said organic solvent or strongly acidic resins in order to to obtain the enol-lactone of 2-oxocyclohexylideneacetic acid which is isolated if desired, BR/ and application to the preparation of 2-coumaranone. / P
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