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The multiplex circulating loop fill device and method for the microanalysis with ion color layer analysis

机译:用于离子色层分析的微分析的多重循环回路填充装置和方法

摘要

(57) Abstract In order to do fixed quantity microanalysis with ion color layer analysis, the minute ion contaminant the ion color layer analytical instrument and the method before on column of making concentrate. This method after making the sample solution the sample fill loop fill up (26), repeats the fact that it removes, includes the continual step of the multiplex circulation which before makes the separated column concentrate (30) cumulatively at the cumulative quantity of the sample. With each removal step, from the sample fill loop (26) pushing out approximately up to 98% of the sample solution of the known quantity the liquid which predetermined time, was pressurized substantially with constant flow facing toward the sample fill loop (26), is included. After that, this the sample solution of the quantity which is investigated passes the ion-exchange resin column (30), the minute ion contaminant is concentrated in the resin.
机译:(57)<摘要>为了用离子色层分析法进行定量的微量分析,在离子色谱层浓缩仪上用离子色层分析仪和以前的方法对微小的离子污染进行了分析。该方法在将样品溶液填充到样品填充环(26)中之后,重复其去除的步骤,包括多重循环的连续步骤,该步骤在使分离的色谱柱(30)累积达到样品的累积量之前是连续的。在每个移除步骤中,从样品填充回路(26)大约以已知量的样品溶液的大约98%推出预定时间的液体,并以恒定的流量朝向样品填充回路(26)进行基本加压,已经包括了。之后,该被研究量的样品溶液通过离子交换树脂柱(30),微小的离子污染物在树脂中浓缩。

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