首页>
外国专利>
Nickel / Calcium Oxide Catalyst for One-Stage Synthesis of Methyl Isobutyl Ketone and Its Manufacturing Method
Nickel / Calcium Oxide Catalyst for One-Stage Synthesis of Methyl Isobutyl Ketone and Its Manufacturing Method
展开▼
机译:一阶段合成甲基异丁基酮的镍/氧化钙催化剂及其制备方法
展开▼
页面导航
摘要
著录项
相似文献
摘要
The present invention relates to a nickel / calcium oxide catalyst which can be used to prepare methyl isobutyl ketone from acetone and hydrogen in one step rather than the conventional three steps, and a method for producing the same. (A) preparing a mixed solution of nickel salts and calcium salts according to the present invention, (b) preparing a gel salt nickel-calcium salt catalyst precursor by evaporating the solvent by heating while stirring the mixed solution, and (c) a simple heat treatment of the catalyst precursor under an atmosphere of 80 to 400 ° C. air or an inert gas for 3 to 12 hours, and then reduction for 1 to 12 hours under a gas atmosphere in which an inert gas and hydrogen are mixed at 400 to 800 ° C. The nickel / calcium oxide catalyst prepared by the process shows much higher catalytic activity than other conventional catalysts in the reaction for producing methyl isobutyl ketone from acetone and hydrogen.
展开▼