首页> 外国专利> LUBE OIL COMPOSITION, OVERBASED ALKALINE EARTH METAL SULFIDE PHENEATE CONCENTRATE USED FOR PREPARING THE SAME, AND PROCESS FOR PREPARING THE CONCENTRATE

LUBE OIL COMPOSITION, OVERBASED ALKALINE EARTH METAL SULFIDE PHENEATE CONCENTRATE USED FOR PREPARING THE SAME, AND PROCESS FOR PREPARING THE CONCENTRATE

机译:润滑油成分,用于制备相同原料的高碱性碱土金属硫化物精矿以及制备精矿的方法

摘要

A lubricating oil composition having a high base value and an excellent high-temperature detergency and comprising an overbased alkaline earth metal phenate sulfide, and a process for producing an overbased alkaline earth metal phenate sulfide having a high base number and a viscosity at 100 DEG C of 1,000 cSt or less and is excellent in hydrolytic stability and oil solubility. And, the overbased alkaline earth metal phenate sulfide concentrate is produced by introducing an alkaline earth metal reagent, a phenol compound in an amount of from 1 to 100 equivalents per mol of the alkaline earth metal reagent, and sulfur into a reactor optionally together with water; adding a dihydric alcohol to the introduced mixture at a pressure inside the reactor of 10 to 250 kPa-G to react them; subsequently distilling off the excess dihydric alcohol and at least the excess amount of the water; treating the resultant bottom residue with carbon dioxide in the presence of from 0.3 to 0.8 mol of water per mol of the alkaline earth metal reagent; causing from 0.001 to 0.3 mol of a fatty acid compound to be present per mol of the alkaline earth metal reagent before the carbon dioxide treatment at the latest; and distilling off the excess phenol compound contained in the product of the carbon dioxide treatment.
机译:具有高碱值和优异的高温去污力并包含高碱性碱土金属酚盐硫化物的润滑油组合物,以及制备高碱性值和在100℃下的粘度的高碱性碱土金属酚盐硫化物的方法1,000 cSt以下,且水解稳定性和油溶性优异。并且,通过将碱土金属试剂,每摩尔碱土金属试剂1至100当量的酚化合物和硫任选地与水一起引入反应器中来生产高碱性碱土金属酚盐硫化物浓缩物。 ;在反应器内的压力为10至250kPa-G的条件下,将二元醇加入到引入的混合物中使它们反应;随后蒸馏出过量的二元醇和至少过量的水;每摩尔碱土金属试剂在0.3至0.8摩尔水的存在下用二氧化碳处理所得的底部残余物;最迟在二氧化碳处理之前使每摩尔碱土金属试剂存在0.001至0.3摩尔脂肪酸化合物;蒸馏出二氧化碳处理产物中所含的过量酚化合物。

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