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Process for the preparation of fabric softeners actives and products that are used.

机译:制备织物柔软剂活性物质和所用产品的方法。

摘要

The invention relates to a method of preparing a biodegradable active agent, fabric softener. Said process comprises the following steps: a) providing a source of triglyceride and reacting said source to form a mixture, comprising FATTY ACIDS FORMULA R 1 CO 2 H, fatty acid esters of the formula R 1 CO 2 R '' '' O mixtures thereof; WHERE R 1 IS ALQ Uilo C 1 - C 22, alkenyl C 2 - C 22, and mixtures thereof; R '' is alkyl C 1 - C 4 hydroxyalkyl MONO C 2 - C 4 dihydroxyalkyl C 3 - C 4; B) RACCIONAR MIXTURE OF PHASE (A) with one or more amines of formula (I), wherein R is alkyl C 1 - C SUB, 6 hydroxyalkyl C 1 - C 6, benzyl or mixtures thereof; Each Z INDEPENDENTLY SELECTED FROM A GROUP CONSISTING - OH, - CHR''OH, - CH (OH) CH 2 OH, NH 2 and mixtures thereof, wherein R '' is C 1 -C 4; M is an integer of 1 to 3; N is an integer of 1 to 4; To form a precursor agent blend fabric softener of formula (II), wherein R, R 1, m and n are the same as defined above; YC) quaternizing said mixture harbinger of step (b) by reacting it with an agent quaternizing OF FORMULA RX, where R is the same as defined in step (B) YX is a compatible anion softener, FORMING AN ACTIVE AGENT SOFTENER TISSUE OF FORMULA (VII), wherein R, R 1, X, Y, m and n are the same as defined Anteri ously; Provided that at least step (C) DEVELOP IN THE PRESENCE OF a chelating agent selected from the group consisting of diethylenetriaminepentaacetic acid, ethylenediamine - N, N 'disuccinic acid and mixtures thereof. SE also provides a method of forming a fabric softener premix AND A fabric softening composition, AND PRODUCTS USED FOR THE THREE STAGES.
机译:本发明涉及一种可生物降解的活性剂,织物柔软剂的制备方法。所述方法包括以下步骤:a)提供甘油三酸酯源并使所述源反应以形成混合物,所述混合物包含脂肪酸配方R 1 CO 2 H,式R 1 CO 2 R'''O的脂肪酸酯混合物其中其中R 1是ALQ Uilo C 1 -C 22,烯基C 2 -C 22及其混合物。 R''是烷基C 1-C 4羟烷基MONO C 2-C 4二羟烷基C 3-C 4; B)阶段(A)与一种或多种式(I)的胺的种族混合物,其中R为烷基C 1 -C SUB,6羟烷基C 1 -C 6,苄基或其混合物;每个Z独立地选自-OH,-CHR''OH,-CH(OH)CH 2 OH,NH 2及其混合物组成的基团,其中R''是C 1 -C 4; M是1至3的整数; N为1〜4的整数。为了形成式(II)的前体剂共混物织物柔软剂,其中R,R 1,m和n与上述定义相同; YC)通过使所述步骤(b)的混合物预混合剂与FORMULA RX季铵化剂反应而季铵化,其中R与步骤(B)中定义的相同。YX是相容的阴离子软化剂,形成配方的活性剂软化剂组织( VII),其中R,R 1,X,Y,m和n与之前定义的相同;只要至少一种步骤(C)存在螯合剂,该螯合剂选自二亚乙基三胺五乙酸,乙二胺-N,N'二琥珀酸及其混合物。 SE还提供了形成织物柔软剂预混合物和织物柔软组合物的方法,以及用于三个阶段的产品。

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