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RECOVERY METHOD OF PLATINUM GROUP METALS FROM SPENT ACTIVE CARBON CATALYST
RECOVERY METHOD OF PLATINUM GROUP METALS FROM SPENT ACTIVE CARBON CATALYST
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机译:活性炭催化剂中铂族金属的回收方法
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摘要
The present invention relates to a method for recovering a platinum group metal from a noble metal-containing activated carbon spent catalyst used in petrochemical or various industries. More particularly, the present invention relates to a waste catalyst containing water and various organic substances, including H 2 O, NaOH, alcohols, and the like. The present invention relates to a method of recovering platinum group metals such as platinum and palladium by completely calcining volatile organic substances and the like remaining in a spent catalyst after washing and removing organic substances using an organic solvent.;As in the recovery method of the present invention, if the organic matter present in the waste catalyst is first removed before the waste catalyst is calcined, it is possible to reduce the occurrence of manure due to incomplete combustion during firing, Losses can also be reduced.;In addition, the platinum group metal mixture obtained after firing is reduced by using a reducing agent such as N 2 H 4 · 2H 2 O or a hydrogen mixed gas, and the platinum group metal is dissolved using various compounds to recover the platinum group metal. It can be obtained in high yield.
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机译:本发明涉及从石油化学或各种工业中使用的含贵金属的活性炭废催化剂中回收铂族金属的方法。更具体地,本发明涉及一种包含水和各种有机物质的废催化剂,所述有机物质包括H 2 Sub 2 O,NaOH,醇等。本发明涉及一种通过在使用有机溶剂洗涤并除去有机物质之后完全煅烧残留在废催化剂中的挥发性有机物质等来回收铂族金属(例如铂和钯)的方法。本发明,如果在煅烧废催化剂之前首先除去废催化剂中存在的有机物,则可以减少由于烧制过程中不完全燃烧引起的粪便的产生,还可以减少损失。使用N 2 Sub> H 4 Sub>·2H 2 Sub> O等还原剂或氢混合气体对烧成后的金属族混合物进行还原。然后使用各种化合物溶解铂族金属以回收铂族金属。可以高产率获得。
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