首页> 外国专利> Transferring device used in analytical measuring techniques comprises temperature-regulated vaporizer with carrier gas feed, gas-tight injection head, column or measuring cell outlet and optionally split outlet

Transferring device used in analytical measuring techniques comprises temperature-regulated vaporizer with carrier gas feed, gas-tight injection head, column or measuring cell outlet and optionally split outlet

机译:分析测量技术中使用的传输设备包括带载气进料的温度调节蒸发器,气密注入头,色谱柱或测量池出口以及可选的分流出口

摘要

A transferring device comprises a temperature-regulated vaporizer with a carrier gas feed, a gas-tight injection head, a column or measuring cell outlet and optionally a split outlet. The heated zones in contact with the sample comprise a chemically inert ceramic body consisting of a single homogeneous compound of group 3a and 4a nitrides, such as boron nitride, aluminum nitride and silicon nitride, or a single homogeneous compound of group 3a and 4a carbides, such as boron carbide, aluminum carbide and silicon carbide or single homogeneous compound of group 3a oxides, such as magnesium oxide and aluminum oxide, or a mixture of the above carbides and oxides, or a composite workpiece made from the above carbides and oxides. The ceramic body has electrically conducting structures for impinging a current. Preferred Features: The ceramic body is made from a powdered starting material produced either by hot pressing or by using nanoparticles having a grain size of less than 100 nm, by cold pressing and subsequently sintering in inert gas in a vacuum at at least 1450 deg C; or is made from pyrolytic nitrides or carbides deposited by CVD/PVD in a vacuum at more than 1500 deg C.
机译:输送装置包括带有载气进料的温度调节蒸发器,气密注入头,色谱柱或测量池出口以及可选的分流出口。与样品接触的加热区包括化学惰性的陶瓷体,该陶瓷体由3a和4a组氮化物的单一均质化合物(例如氮化硼,氮化铝和氮化硅)或3a和4a组碳化物的单一均质化合物组成,例如碳化硼,碳化铝和碳化硅,或3a族氧化物的单一均质化合物,例如氧化镁和氧化铝,或上述碳化物和氧化物的混合物,或由上述碳化物和氧化物制成的复合工件。陶瓷体具有用于传导电流的导电结构。优选特征:陶瓷体由粉末状原料制成,该粉末状原料通过热压或通过使用粒度小于100nm的纳米颗粒,冷压并随后在惰性气体中在至少1450℃下烧结而制得。 ;或由在1500摄氏度以上的真空中通过CVD / PVD沉积的热解氮化物或碳化物制成。

著录项

  • 公开/公告号DE10136594A1

    专利类型

  • 公开/公告日2003-03-13

    原文格式PDF

  • 申请/专利权人 PAPLEWSKI MARTIN;

    申请/专利号DE2001136594

  • 发明设计人 PAPLEWSKI MARTIN;

    申请日2001-07-29

  • 分类号G01N30/12;G01N1/28;

  • 国家 DE

  • 入库时间 2022-08-21 23:42:45

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