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PROCESS FOR THE PREPARATION OF ODOUR-LEAN POLYETHER POLYOLS

机译:制备稀薄聚酯树脂的方法

摘要

A process for the preparation of odor-lean polyether polyols from polyether polyol product stream obtained by reacting a starting compound having a plurality of active hydrogen atoms with one or more alkylene oxides, which process comprises the steps of: (a) contacting the polyether polyol product with an excess of acid having a pKa of less than 5 under hydrolysis conditions, (b) contacting the reaction mixture with excessive amount of water to form a two-phase system under hydrolysis conditions by adding an amount of water to form an organic phase and a water phase to reduce the amount of cyclic-ether compounds present in the polyether polyol product, and (c) recovering the odor-lean polyether polyol.
机译:一种由具有多个活性氢原子的起始化合物与一种或多种环氧烷反应制得的聚醚多元醇产物流制备无味聚醚多元醇的方法,该方法包括以下步骤:(a)使聚醚多元醇接触水解条件下,pKa小于5的酸的过量产物;(b)在水解条件下,通过添加一定量的水以形成有机相,使反应混合物与过量的水接触以形成两相体系用于减少聚醚多元醇产物中存在的环醚化合物的量的水相;和(c)回收无气味的聚醚多元醇。

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