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METHOD OF DETERMINING O- AND M-NITROTOLUENES IN AIR

机译:空气中邻硝基甲苯和间硝基甲苯的测定方法

摘要

FIELD: analytical methods.;SUBSTANCE: determination of o- and m-nitrotoluenes in air comprising sampling, modifying piezosensor with active sorbent, passing sample along with carrying gas through detection cell, and recording piezosensor signal is characterized by that active sorbent utilized is triton X-100 taken in amount 10-12 mcm, carrying gas is air, which is passed through detection cell before passage of sample, and passage velocity and passage time in both cases are 45-55 cm3/min and 2-3 min. Advantages of the method are: essentially simplified analytical equipment, diminished analysis and modification times, reduced number reagents utilized, lowered determination temperature from 210оС to 20-25оС.;EFFECT: accelerated analytical procedure and reduced expenses.;2 tbl, 7 ex
机译:领域:分析方法;物质:测定空气中的邻硝基甲苯和间硝基甲苯,包括取样,用活性吸附剂修饰压电传感器,将样品与运载气体一起通过检测单元并记录压电传感器信号,其特征在于所使用的活性吸附剂为triton X-100的量为10-12 mcm,载气为空气,在样品通过之前先通过检测池,两种情况下的通过速度和通过时间均为45-55 cm3 / min和2-3 min。该方法的优点是:实质上简化了分析设备,减少了分析和修改时间,减少了使用的试剂数量,将测定温度从210°C降低到20-25°C。效果:加速了分析过程并降低了费用。

著录项

  • 公开/公告号RU2237893C2

    专利类型

  • 公开/公告日2004-10-10

    原文格式PDF

  • 申请/专利权人

    申请/专利号RU20020132774

  • 申请日2002-12-05

  • 分类号G01N30/00;G01N31/00;C07C205/06;

  • 国家 RU

  • 入库时间 2022-08-21 22:44:51

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