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DEVICE FOR GC analysis concentrations of carbon monoxide and methane in multicomponent mixtures

机译:用于多组分混合物中一氧化碳和甲烷浓度的GC分析装置

摘要

The invention relates to analytical chemistry, in particular to a gas chromatography, and can be used in the laboratories of chemical plants, research laboratories, analysis of environmental pollution, petroleum products and so forth. In an apparatus for gas chromatographic analysis of carbon dioxide concentration and methane multicomponent mixtures comprising series-connected feeder for the injection, the chromatographic column filled with the stationary phase and the detector, according to useful mode if, before dosing the injection series along the carrier gas motion mounted stabilizer of carrier gas pressure, pressure gauge, variable inductors in parallel with each other and three-way cock, and the chromatographic column is further installed threeway cock and the detection unit comprising a measuring and comparative camera. The stationary phase of the chromatographic column comprises a granular activated with a grain size of 0.3-0.5 mm. In this chromatographic column formed 1200-1300 mm in length with a diameter of 2.95-3.05 mm. The measuring chamber is installed with a thermal conductivity detector operating current of 100-101 mA. As a carrier gas hydrogen is used under pressure 0,24-0,25 kg / cm 3 at a flow rate 2-2.1 L / h.
机译:本发明涉及分析化学,尤其涉及一种气相色谱,可用于化工厂实验室,研究实验室,环境污染分析,石油产品等。在用于气相色谱分析二氧化碳浓度和甲烷多组分混合物的设备中,该设备包括用于进样的串联连接的进料器,如果在沿着进样器进样进样系列之前,根据有用模式,色谱柱装有固定相和检测器气体运动安装的载气稳定器,压力表,可变电感器和三通旋塞相互并联,色谱柱还安装了三通旋塞,检测单元包括一个测量和比较摄像机。色谱柱的固定相包含粒度为0.3-0.5毫米的活化颗粒。在该色谱柱中形成的长度为1200-1300mm,直径为2.95-3.05mm。测量室安装有100-101 mA的热导检测器。作为载气,氢气在压力0.24-0.25 kg / cm 3 下以2-2.1 L / h的流量使用。

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