The integrated system of polymerization in laboratory scale and method.

摘要

"The integrated system of polymerization in laboratory scale and method.It is described an integrated system of polymerization in laboratory scale, preferably suitable for polymerization and / or copolymerization mass or solution of styrene and its derivatives.Allowing the addition of rubber, comonu00f3meros, flow aids and additives in general.The integrated system comprises at least one reactor (101) of the mixture and polymerization monomers fed in by a line (109), with control of agitation (104).Pressure indicator (102) and temperature (103), a reactor (201) connected to the reactor for the polymerization isotermicamente (101) by a line (113), also equipped with control of agitation (204).Pressure indicators (202), and temperature (203), a reactor (201) being connected via the line (212) is a devolatilizador (301) connected to a vacuum pump (303).Traps and heating system (308).The devolatilizador (301) being provided with removable lid (302) for introduction of the polymeric material in the tubes (309) to complete the conversion and devolatilizar polymeric mass.And then analyze it.In an alternate configuration.The integrated system includes an additional reactor (401) for mixing and / or polymerization connected to the reactor (201) via the line (412) is also described the method to operate the integrated system.