首页> 外国专利> METHOD OF MAKING PHOTOCATALYSTS BY LOADING TITANIUM DIOXIDE FILM ON FLEXIBLE SUBSTRATES

METHOD OF MAKING PHOTOCATALYSTS BY LOADING TITANIUM DIOXIDE FILM ON FLEXIBLE SUBSTRATES

机译:通过将二氧化钛薄膜负载在柔性基底上来制造光催化剂的方法

摘要

The photocatalyst titanium dioxide film of disclosed method preparation is included the following steps: that (1) prepares active layer sol, passed through by the method in flexible substrate: (a) preparation includes tetrabutyl titanate, ethyl alcohol, diethanol amine and water; (2) pore creating material is added and is selected from polyethylene glycol, octadecylamine and its mixture and precursor solution; (3) obtained solution is placed in closed gelatinization process at least 33 days; (2) prepare active tio2 photocatalyst layer by: (one) coating flexible substrate and active layer sol preparation according to step (1) using lifting and be coated with process; (2) flexible base board of dry coating; (3) coating, dry flexible substrates are put into water heating kettle, for thermal crystallization second alcohol and water in the mixed solvent at 60-200 °C. Further disclosed method, wherein precursor solution be include titanium tetrachloride, second alcohol and water.
机译:本发明方法制备的光催化剂二氧化钛薄膜包括以下步骤:(1)制备活性层溶胶,通过该方法在柔性基材上通过:(a)制备包括钛酸四丁酯,乙醇,二乙醇胺和水; (2)加入造孔材料,其选自聚乙二醇,十八烷基胺及其混合物和前体溶液; (3)将获得的溶液置于密闭糊化过程中至少33天; (2)通过以下步骤制备活性二氧化钛光催化剂层:(一)使用提拉方法按照步骤(1)涂覆柔性基材和活性层溶胶制备方法并进行涂覆; (2)干涂柔性基板; (3)将涂料,干燥的柔性基材放入水热釜中,使第二醇和水在混合溶剂中于60-200°C进行热结晶。进一步公开了方法,其中前体溶液包括四氯化钛,第二醇和水。

著录项

  • 公开/公告号EP1531930A1

    专利类型

  • 公开/公告日2005-05-25

    原文格式PDF

  • 申请/专利权人 TSINGHUA UNIVERSITY;

    申请/专利号EP20030763572

  • 发明设计人 HE YU;YU FANG;ZHU YONGFA;

    申请日2003-07-11

  • 分类号B01J21/06;

  • 国家 EP

  • 入库时间 2022-08-21 22:07:39

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