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Blue dye with particularly high purity and positive triboelectric control effect

机译:蓝色染料具有极高的纯度和积极的摩擦电控制作用

摘要

The dye base sulphate of formula (I) is produced with a residual amine content of less than 2000 ppm, as determined by HPLC, by precipitation of the dye base, made by Friedel-Crafts alkylation, substitution and hydrolysis, as the dye base sulphate and a) taken up in water and subjecting to a first steam distillation then filtered and optionally dried at 50 to 180° C., b) the pressed cake is treated with water or the optionally dried dye base sulphate is moistened with water, c) subjected to a further steam distillation and filtration and d) dried at 50 to 180° C.
机译:通过HPLC测定,通过由Friedel-Crafts烷基化,取代和水解制备的染料碱的沉淀,产生具有小于2000ppm的残留胺含量的式(I)的染料基础硫酸盐,作为染料基础硫酸盐。 a)吸收在水中并进行第一次蒸汽蒸馏,然后过滤,并任选在50至180°C下干燥,b)压滤饼用水处理或将任选干燥的染料基础硫酸盐用水润湿,c)进行进一步的蒸汽蒸馏和过滤,并且d)在50至180℃下干燥。

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