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METHOD FOR THE EVALUATION OF THE AROMA OF TOBACCO SMOKE AND CLASSIFICATION BY AROMA OF TYPES AND VARIETIES OF TOBACCOS

机译:烟熏香气的评估方法及按烟种和品种的香气进行分类

摘要

The method is used for objective numerical evaluation of the aroma of tobacco smoke of Oriental tobaccos and offers a chance for the classification by aroma of the types and varieties of Oriental and Virginia type tobaccos. A sample of dry, ground tobacco is subjected to analysis for the content of isovalerianic acid and the neutral fraction of essential oil by means of capillary gas chromatography, after which the aroma (A) is determined according to the formula A = 0.0946 x [Kisoval.] + 15.547, and the pleasure of aroma (A') by formula A' = 0.0156 x [Kisoval.] + 5.7448 wherein [Kisoval.] means the isovalerianic acid concentration in the sample, expressed in microg.g -1. The numerical values produced are related to reference scales expressing the aroma, as follows: highly aromatic tobacco smoke - mark over 20, medium aromatic tobacco smoke - mark 20, low aromatic tobacco smoke - mark under 20; and for the pleasure of the aroma, as follows: highest pleasure of the tobacco smoke aroma - mark 10; the lowest tobacco smoke aroma - marks 1 to 5, and intermediate pleasure of the tobacco smoke aroma - marks between 5 and 7. The aroma classification is made by processing of the chromatographic profiles of the chromatographic analysis of the neutral fraction of the essential oil based on the time of retention of each peak (tR) and the percentage participation of the height (H) of each peak from the sum of heights of the selected peaks in the processing of all chromatogrammes. The results are expressed by indexes of similarity (Is, %) between the compared samples. The classification is made on the aroma of tobacco smoke selected for reference value, the Is of which is taken for 100%, or by the comparison of the different tobaccos amongst them.
机译:该方法用于客观评价东方烟草烟气的香气,为通过香气对东方和弗吉尼亚型烟草的种类和品种进行分类提供了机会。通过毛细管气相色谱法对干燥的磨碎烟草样品进行异戊酸含量和精油中性成分分析,然后根据公式A = 0.0946 x [Kisoval ] +15.547,和通过式A′获得的香气(A′)的愉悦度= 0.0156×[Kisoval。] + 5.7448,其中[Kisoval。]是指样品中异戊酸的浓度,以微克-1表示。产生的数值与表示香气的参考标度相关,如下:高芳香性烟草烟雾-超过20分,中芳香性烟草烟雾-达到20分,低芳香性烟草烟雾-低于20分;为了使香气愉悦,如下:烟草烟气香气的最高愉悦感-满分10;最低的烟草烟雾香气-标记1到5,以及中等程度的烟草烟雾香气-标记在5到7之间。通过处理精油中性馏分的色谱分析的色谱图进行香气分类每个色谱图的保留时间(tR)和每个峰的高度(H)与所选峰的高度之和的参与百分比。结果由比较样品之间的相似性指数(Is,%)表示。根据选择作为参考值的烟草烟雾的香气进行分类,Is为100%,或通过比较其中的不同烟草而得出。

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