首页> 外国专利> Process for purification of a monomu00earo by extraction with a training officer of the phases and crystallization, the use of monu00c8meros obtained and device su00ecntese

Process for purification of a monomu00earo by extraction with a training officer of the phases and crystallization, the use of monu00c8meros obtained and device su00ecntese

机译:通过与有关人员进行阶段纯化和结晶提纯来纯化单体的方法,使用所获得的单体并使用装置

摘要

Process for purification of a monu00c8mero by extraction with a training officer of the phases and crystallization, the use of monu00c8meros obtained and device su00ecntese ".The invention relates to a process for purification of an acid monomer having a double bond, comprising the steps of: (a) providing a mixture of departure.Containing as components of the mixture of departure, respectively, based on the mixture of departure: (A1) at least 5% by weight of monomer acid; and (A2) at least 0,01% by weight of water, or (A3) at least 0.01% by weight of at least one component of the mixture of departure; or (A2) and (A3).In which the sum of fractions in% by weight of the components of the mixture of departure is respectively 100% by weight; (b) adding an agent forming phases, or a salt of the training officer of phases.Or a mixture of both, to obtain a mixture of purification.Of which: (c) at least one first phase and at least one another phase different from the first stage with a limit of phases form a system of phases; (d) to reduce the temperature of the system of stages.Where: (E) in one of the phases of the system phases, a crystal product containing at least 50% by weight of the components of the mixture of departure is formed, and another component of the mixture of departure.As a crystalline system; and (f) isolation of the crystal product, as well as a device for synthesis of a monomer acid having a double bond.A process for producing an acid monomer having a double bond, a monomer having a double bond and acid obtainable by this process, fibers, films, foams, bodies formed.Superabsorbent polymers and other polymers to the base or acid containing the monomer, the use of acid monomer in or for the production of fibers, films, foams, bodies formed.Superabsorbent polymers or other specialty polymers.
机译:通过培训人员提取各相和结晶来纯化mon u00c8mero的方法,使用获得的mon u00c8meros和装置的方法。本发明涉及具有双重结构的酸单体的纯化方法。键,包括以下步骤:(a)提供离去混合物。基于离去混合物分别包含离去混合物作为组分:(A1)至少5%重量的单体酸;和(A2 )至少0.01重量%的水,或(A3)至少0.01重量%的离开混合物的至少一种组分;或(A2)和(A3)。离开混合物的成分按重量计分别为100%;(b)添加形成剂的相或相的训练人员的盐,或两者的混合物,以获得纯化的混合物。其中:(c)至少一个第一阶段和至少一个不同于第一阶段的其他阶段,且有限制阶段构成阶段系统; (d)降低各阶段系统的温度。其中:(E)在该系统阶段的各相中,形成一种晶体产物,该晶体产物含有至少50重量%的离开混合物的组分,和离开混合物的另一个组成部分。作为晶体系统; (f)结晶产物的分离,以及具有双键的单体酸的合成装置。一种具有双键的酸单体的制造方法,具有双键的单体和可通过该方法得到的酸,纤维,薄膜,泡沫,物体形成的超吸收性聚合物和其他聚合物,以含单体的酸或酸为基础,使用酸性单体生产或制造纤维,薄膜,泡沫,物体形成的超吸收性聚合物或其他特种聚合物。

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