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carbon nanostructures and process for producing nanotubes, nanofibers and carbon based nanostructures

机译:碳纳米结构及生产纳米管,纳米纤维和碳基纳米结构的方法

摘要

"Carbon nanostructures and process for the production of carbon-based nanotubes, nanofibers and nanostructures". The present invention relates to a continuous process for producing carbon-based nanotubes, nanofibers and nanostructures, comprising the following steps: generating an electrically powered plasma, introducing a carbon precursor and / or one or more catalysts and / or a carrier plasma gas in a reaction zone of a high temperature resistant airtight vessel optionally having a thermal insulation liner, vaporize the carbon precursor in the reaction zone at a very high temperature, preferably 4000 198 C or more. drive the plasma vehicle gas, the vaporized carbon precursor and the catalyst through a nozzle whose diameter is narrowing in the direction of the plasma gas flow, conduct the vehicle plasma gas, the vaporized carbon precursor and the catalyst in a blast cooling zone for nucleation, growth and blast-cooling operation with flow conditions generated by aerodynamic forces and electromagnet so that there is no significant recirculation of raw materials and products from the blast zone in the reaction zone, control the gas temperature in the blast zone between about 4000 198 C at the top of that zone and about 50 198 C at the bottom of that zone and control the blast cooling speed between 10¬ 4¬3 K / s and 10¬ 6¬ K / s, blast and extract nanotubes, nanofibers and other nanostructures based on carbon from the blast cooling zone, separate nanotubes, nanofibers and carbon-based nanostructures from other reaction products.
机译:“碳纳米结构和碳基纳米管,纳米纤维和纳米结构的生产方法”。本发明涉及用于生产碳基纳米管,纳米纤维和纳米结构的连续方法,其包括以下步骤:产生电动等离子体,将碳前体和/或一种或多种催化剂和/或载体等离子体气体引入到碳纳米管中。任选具有隔热衬里的耐高温气密容器的反应区在非常高的温度下,优选在4000℃或更高的温度下蒸发反应区中的碳前体。通过直径在等离子气流方向上变窄的喷嘴驱动等离子车辆气体,气化碳前驱体和催化剂,在鼓风冷却区中引导车辆等离子气体,气化碳前驱体和催化剂成核,空气动力学力和电磁体产生的流动条件来进行鼓风和鼓风冷却操作,从而使反应区高炉区的原料和产品没有明显的再循环,将高炉区的气体温度控制在约4000 <198>在该区域的顶部C和在该区域的底部约50 <198> C,并控制喷砂冷却速度在10¬4‑3 K / s和10¬6¬K / s之间,喷砂和提取纳米管,纳米纤维以及来自鼓风冷却区的基于碳的其他纳米结构,与其他反应产物分离的纳米管,纳米纤维和基于碳的纳米结构。

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