首页> 外国专利> METHOD FOR THE CONTINUOUS PRODUCTION OF A COMPOUND THAT CARRIES AT LEAST TWO FUNCTIONAL GROUPS.

METHOD FOR THE CONTINUOUS PRODUCTION OF A COMPOUND THAT CARRIES AT LEAST TWO FUNCTIONAL GROUPS.

机译:连续产生至少两个功能组的化合物的方法。

摘要

The invention relates to a method for the continuous production of a compound that carries at least two functional groups, independently selected from the group consisting of nitrile group, carboxylic acid group, carbonic ester group, carbonic amide group. The inventive method comprises the following steps: a) adding two terminal olefins that carry the functional groups required for the production of the compound according to a1) carrying at least two functional groups, in the presence of a compound according to a3) that is suitable as a catalyst for said addition and that is homogenous with respect to the reaction mixture, thereby obtaining a mixture that contains a1) a compound obtained by simple addition of the two above-mentioned terminal olefins that carry at least two functional groups, independently selected from the group consisting of nitrile group, carboxylic acid group, carbonic ester group, carbonic amide group, a2) a compound obtained by multiple addition of the above-mentioned two terminal olefins, and a3) the compound that is suitable as a catalyst for said addition and that is homogenous with respect to the reaction mixture, b) distilling the mixture obtained in step a) while obtaining b1) the compound obtained by simple addition of the two above-mentioned terminal olefins that carry at least two functional groups, independently selected from the group consisting of nitrile group, carboxylic acid group, carbonic ester group, carbonic amide group, as the overhead product, and b2) a mixture containing b2a) a compound obtained by simple addition of the two above-mentioned terminal olefins that carry at least two functional groups, independently selected from the group consisting of nitrile group, carboxylic acid group, carbonic ester group, carbonic amide group, b2b) a compound obtained by multiple addition of the above-mentioned two terminal olefins, and b2c) the compound that is suitable as a catalyst for said addition and that is homogenous with respect to the reaction mixture, c) separating the entire mixture obtained in step b2) or a part thereof by means of a semipermeable membrane while obtaining a permeate and a retentate in such a manner that the weight ratio of component b2b) to component b2c) of the mixture added in step c) is smaller than in the retentate, d) returning, either partially or completely, to step a) the permeate obtained in step c), and e) returning, either partially or completely, to step a) the part of the mixture obtained in step b2) and not separated according to step c).
机译:本发明涉及一种连续生产带有至少两个官能团的化合物的方法,所述官能团独立地选自腈基,羧酸基,碳酸酯基,碳酸酰胺基。本发明的方法包括以下步骤:a)在合适的根据a3)的化合物的存在下,添加两个携带有生产根据a1)的化合物所需的官能团的末端烯烃,所述带有至少两个官能团的化合物作为用于所述加成反应的催化剂,并且相对于反应混合物是均相的,从而获得包含以下化合物的混合物:a1)通过简单地加成两个上述带有至少两个官能团的末端烯烃的化合物,所述独立地选自由腈基,羧酸基,碳酸酯基,碳酸酰胺基组成的组,a2)通过上述两个末端烯烃的多次加成获得的化合物,和a3)适合作为所述加成催化剂的化合物并且相对于反应混合物是均匀的,b)蒸馏步骤a)中获得的混合物,同时获得b1)通过简单方法获得的化合物带有至少两个官能团的上述两个末端烯烃的加成产物作为塔顶产物,其独立地选自腈基,羧酸基,碳酸酯基,碳酸酰胺基,和b2) b2a)通过简单地添加上述两个带有至少两个官能团的末端烯烃而获得的化合物,所述官能团独立地选自腈基,羧酸基,碳酸酯基,碳酸酰胺基,b2b)通过多次加入上述两个末端烯烃而获得,b2c)适于作为所述加入的催化剂并且相对于反应混合物是均相的化合物,c)分离在步骤b2)中获得的全部混合物或通过半透膜的一部分,同时获得渗透物和截留物,使得组分b2b)与组分b2c)的重量比为o如果在步骤c)中添加的混合物小于截留液中的混合物,d)部分或全部返回步骤a)步骤c)中获得的渗透物,以及e)部分或全部返回步骤a)在步骤b2)中获得的并且没有根据步骤c)分离的混合物的一部分。

著录项

  • 公开/公告号MXPA05013187A

    专利类型

  • 公开/公告日2006-03-09

    原文格式PDF

  • 申请/专利权人 BASF AKTIENGESELLSCHAFT;

    申请/专利号MX2005PA13187

  • 发明设计人 WOLFRAM STUER;

    申请日2004-06-11

  • 分类号C07C51/353;C07C67/303;C07C67/347;C07C67/56;C07C69/593;

  • 国家 MX

  • 入库时间 2022-08-21 21:38:31

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