首页> 外国专利> METHOD FOR DEFINITION OF CONCENTRATION OF TRINITROTOLUENE AND AMMONIUM NITRATE IN AQUEOUS SOLUTIONS FORMED AFTER EXTRACTION OF AMOTOL FROM AMMUNITIONS BEING UTILIZED

METHOD FOR DEFINITION OF CONCENTRATION OF TRINITROTOLUENE AND AMMONIUM NITRATE IN AQUEOUS SOLUTIONS FORMED AFTER EXTRACTION OF AMOTOL FROM AMMUNITIONS BEING UTILIZED

机译:测定从弹药中提取苯甲酰胺后制成的水溶液中三硝基甲苯和硝酸铵浓度的方法

摘要

The utility model relates to analytical chemistry. A method for definition of concentration of trinitrotoluene and ammonium nitrate in aqueous solutions formed after extraction of amatol from ammunitions being utilized comprises direct areomectric definition of ammonium nitrate density and photocolorimetry of colored solution of trinitrotoluene adduct with sodium sulfite. For the definition of ammonium nitrate solution and concentration of trinitrotoluene the explosive is preliminarily extracted from the solution of ammonium nitrate by a method of extraction, and the extraction is carried out by chloroform. After separation of extragent trinitrotoluene is dissolved in ethyl alcohol with subsequent dilution of extract with water for photocolorimetry of alcoholic and aqueous solution.
机译:本实用新型涉及分析化学。定义从使用的弹药中提取氨苯酚后形成的水溶液中三硝基甲苯和硝酸铵浓度的方法,包括硝酸铵密度的直接等电比重测定和亚硫酸钠与三硝基甲苯加合物的有色溶液的光度法。为了定义硝酸铵溶液和三硝基甲苯的浓度,先用提取方法从硝酸铵溶液中提取炸药,然后用氯仿提取。分离出萃取剂后,将三硝基甲苯溶于乙醇,然后用水稀释萃取液,用于酒精和水溶液的光度法测定。

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