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METHOD FOR PRODUCING DIARYLETHENE COMPOUND AND NOVEL DIARYLETHENE COMPOUND

机译:二芳基醚化合物和新型二芳基醚化合物的制备方法

摘要

Disclosed is a method for safely and efficiently producing a diarylethene with high yield without using a special cooling device and the like. Specifically disclosed is a method for producing a diarylethene compound which is characterized in that a lithium compound solution and an alkene compound solution are introduced into a microreactor having a channel where a plurality of liquids can be mixed, and a lithium compound and an alkene compound are subjected to a cross-coupling reaction in the microreactor. A cycloalkene compound represented by the structural formula (II) below is preferable as the alkene compound. Structural formula (II) In the structural formula (II), n represents an integer of 2-5; X represents hydrogen, chlorine or fluorine; and Y represents a halogen atom.
机译:本发明公开了一种不使用特殊的冷却装置等而安全且有效地高收率地生产二芳基乙烯的方法。具体地公开了一种制备二芳基乙烯化合物的方法,其特征在于将锂化合物溶液和烯烃化合物溶液引入具有可混合多种液体的通道的微型反应器中,并且锂化合物和烯烃化合物为在微反应器中进行交叉偶联反应。由以下结构式(II)表示的环烯烃化合物优选作为烯烃化合物。结构式(II)在结构式(II)中,n表示2-5的整数。 X代表氢,氯或氟; Y表示卤原子。

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