首页> 外国专利> THE PROCESSING METHOD OF HIGH IONIC CONDUCTING SCANDIA STABILIZED ZIRCONIA AND SCANDIA STABILIZED ZIRCONIA ELECTROLYTE

THE PROCESSING METHOD OF HIGH IONIC CONDUCTING SCANDIA STABILIZED ZIRCONIA AND SCANDIA STABILIZED ZIRCONIA ELECTROLYTE

机译:高离子传导斯堪迪亚稳定氧化锆和斯堪迪亚稳定化氧化锆电解质的制备方法

摘要

A method for preparing a highly ion conductive Scandia stabilized zirconia, and a method for preparing an electrolyte by using the Scandia stabilized zirconia are provided to simplify the manufacturing process, to improve ion conductivity, thereby enhancing the performance of a fuel cell, and to allow the material to be sintered at a lower temperature, thereby reducing a manufacturing cost. A method for preparing a highly ion conductive Scandia stabilized zirconia comprises the steps of weighing scandium nitrate (Sc(NO3)3.5H2O) and zirconium nitrate (ZrO(NO3)2.2H2O) so as to make the ratio of scandium and zirconium be 8-9 : 91-92 or 10-11 : 81-90 by mol, dissolving them in distilled water, and adding glycine; heating the obtained solution at 90-100 deg.C and stirring it to evaporate water; increasing the heating temperature to 200-250 deg.C to obtain an powder by self-complexation; and calcining it at 650-750 deg.C for 1-3 hours.
机译:提供一种用于制备高离子导电性的斯堪的纳维亚稳定的氧化锆的方法,以及通过使用该斯堪的亚稳定化的氧化锆制备电解质的方法,以简化制造工艺,提高离子电导率,从而增强燃料电池的性能,并允许该材料将在较低的温度下烧结,从而降低了制造成本。一种制备高离子导电性的dia离子稳定的氧化锆的方法包括称重硝酸scan(Sc(NO3)3.5H2O)和硝酸锆(ZrO(NO3)2.2H2O)的步骤,以使of与锆之比为8。 9:91-92或10-11:81-90,以摩尔计,将它们溶解在蒸馏水中,并加入甘氨酸。将获得的溶液在90-100℃下加热并搅拌以蒸发水。将加热温度升高至200-250℃,通过自络合得到粉末。并在650-750℃下煅烧1-3小时。

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