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SYNTHESIS OF TOURMALINE RED COLORED CUBIC ZIRCONIA SINGLE CRYSTALS

机译:电气石红色彩色立方氧化锆单晶的合成

摘要

A manufacturing method of a tourmaline red colored cubic zirconia single crystal is provided to enable mass production and improve quality by adding MnO2 to the material of the crystal as a color developer and performing a heat-treatment in a neutral or reduction atmosphere. A manufacturing method of a tourmaline red colored cubic zirconia single crystal includes the steps of: mixing an oxide material; charging a skull melting apparatus with a compound obtained from the prior step, and growing a zirconia single crystal with a skull melting method; and performing the heat-treatment of the single crystal at the temperature of 950 - 1500 degrees centigrade in a furnace of a neutral or reduction atmosphere. The oxide material includes ZrO2 of 50 - 90 weight%, Y2O3 of 10 - 50 weight%, CeO2, Er2O3, a color former of 0.02 - 9 weight%, and MnO2 of 0.01 - 4 weight% as a color developer. The color developer is added less than half of the color former.
机译:提供一种电气石红色立方氧化锆单晶的制造方法,其通过将MnO 2作为显色剂加入到晶体材料中并在中性或还原性气氛中进行热处理,从而能够大量生产并提高质量。电气石红色立方氧化锆单晶的制造方法包括以下步骤:混合氧化物材料;和向颅骨熔化设备中装入从先前步骤获得的化合物,并通过颅骨熔化方法生长氧化锆单晶。在中性或还原性气氛的炉中在950-1500摄氏度的温度下对单晶进行热处理。所述氧化物材料包括50-90重量%的ZrO 2,10-50重量%的Y 2 O 3,CeO 2,Er 2 O 3,0.02-9重量%的成色剂和0.01-4重量%的MnO 2作为显色剂。显色剂的添加量少于成色剂的一半。

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