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Ion Mobility Spectrometer Comprising a Corona Discharge Ionization Element

机译:包含电晕放电电离元素的离子迁移谱仪

摘要

An ion mobility spectrometer is disclosed wherein the ionization element is a corona discharge source (300) consisting of: a first chamber (308) provided with an inlet (309) for a gas to be analyzed and with at least one first opening (311) for communication between the internal space of the first chamber and the reaction zone of the spectrometer; a second chamber (303), contained in the first chamber, provided with an inlet (306) for an ultra-pure gas or a mixture of ultra-pure gases, and with at least one second communication opening (310, 310′) between the first and the second chamber; a pair of electrodes (304, 302′), at least one of which (304) is needle-shaped, arranged in the second chamber, with the pair of electrodes and the second opening arranged in such geometrical relationships that there is no optical path between the zone of the corona discharge and the ion detector of the IMS instrument. The instrument of the invention allows to reproduce the results of a spectrometer equipped with a 63Ni ionization source, while avoiding the problems connected to the transportation and use of radioactive material.
机译:公开了一种离子迁移谱仪,其中所述电离元件是电晕放电源( 300 ),该电晕放电源包括:第一腔室( 308 ),该腔室设有入口( 309) )用于分析的气体,并具有至少一个第一开口( 311 ),用于在第一腔室的内部空间和光谱仪的反应区之间进行连通;包含在第一腔室中的第二腔室( 303 )设有用于超纯气体或超纯气体混合物的入口( 306 ),以及在第一腔室和第二腔室之间具有至少一个第二连通开口( 310、310 ');一对电极( 304、302 ')(其中至少一个( 304 )是针状的)布置在第二腔室中,该对电极和第二开口的几何关系使得电晕放电区域与IMS仪器的离子检测器之间没有光路。本发明的仪器允许再现配备有 63 Ni电离源的光谱仪的结果,同时避免了与放射性物质的运输和使用有关的问题。

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