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NMR spectrometer with common refrigerator for cooling an NMR probe head and cryostat

机译:带有普通制冷机的NMR光谱仪,用于冷却NMR探头和低温恒温器

摘要

An NMR apparatus comprising a superconducting magnet coil system, in particular, an NMR spectrometer, with a cryostat which comprises an outer shell and a helium tank which contains the magnet coil system, and with an NMR probe head which is disposed in a room temperature bore of the cryostat and which contains a cooled RF resonator for receiving NMR signals from a sample to be examined and is cooled, together with the NMR probe head, by a cold head of a common, multi-stage, compressor-operated refrigerator, is characterized in that the cold head of the refrigerator is disposed in a neck tube, the upper end of which is connected to the outer shell of the cryostat and the lower end of which is connected to the helium tank in such a manner that the neck tube and the helium tank delimit a helium space, with at least one cooling circuit with thermally insulated transfer lines being provided between the helium space and the NMR probe head, wherein the cryogenic helium in the helium space is used as coolant for the cooling circuit. This produces an NMR apparatus which cools a plurality of elements at different temperature levels using only one single cryocooler to optimally utilize the cooling resources of the refrigerator.
机译:NMR设备,包括超导磁体线圈系统(特别是NMR光谱仪),具有恒温器的低温恒温器,该低温恒温器包括一个外壳和一个容纳该电磁线圈系统的氦气罐,以及一个NMR探头,该探头放置在室温孔中低温恒温器的特征在于,它包含一个冷却的RF谐振器,用于接收来自待检查样品的NMR信号,并与NMR探头一起由一台普通的多级压缩机操作式冰箱的冷头冷却。因为冰箱的冷头设置在颈管中,其上端与低温恒温器的外壳相连,而其下端则与氦气罐相连,从而使颈管和氦气罐界定了一个氦气腔,在氦气腔和NMR探头之间设有至少一个带有绝热传输线的冷却回路,其中氦气腔中的低温氦气为用作冷却回路的冷却剂。这产生了一种NMR设备,该NMR设备仅使用一个低温冷却器就可以在不同的温度水平下冷却多个元件,以最佳地利用冰箱的冷却资源。

著录项

  • 公开/公告号US7430872B2

    专利类型

  • 公开/公告日2008-10-07

    原文格式PDF

  • 申请/专利权人 MARCO STROBEL;

    申请/专利号US20050281442

  • 发明设计人 MARCO STROBEL;

    申请日2005-11-18

  • 分类号F25B19/00;F25B19/02;F25D23/12;

  • 国家 US

  • 入库时间 2022-08-21 20:10:34

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