首页> 外国专利> AN IMPROVED PROCESS FOR THE EXTRACTION OF EPHEDRINE HYDROCHLORIDE FROM EPHEDRA GERARDIENA

AN IMPROVED PROCESS FOR THE EXTRACTION OF EPHEDRINE HYDROCHLORIDE FROM EPHEDRA GERARDIENA

机译:一种从麻黄加倍体中提取盐酸盐酸表麻碱的改进方法

摘要

An improved process for the extraction of epherdrine hydrochlo ride from Ephedra gerardiena which comprises steam distilling powdered ephedra herb in presence of alkali and adjusting the pH of of the distillate in the range of 4.5 to 605, concentrating the said distillate and adjusting pH in the range of 7 to 10 then Saturating with sodium chloride and extracting with organic solvent such as herein described removing the said solvent, to obtain crude alkaloids then treating with alcoholic hydrochloric acid in conventional manner followed by crystallisation to obtain ephedrine hydrochloride.
机译:一种改进的从麻黄中提取盐酸麻黄碱的方法,该方法包括在碱存在下蒸汽蒸馏麻黄粉末,并将馏出物的pH调节至4.5至605,浓缩所述馏出物并调节pH在该范围内。将其在7至10中溶解,然后用氯化钠饱和,并用本文所述的有机溶剂萃取,除去所述溶剂,得到粗生物碱,然后以常规方式用醇盐酸处理,再结晶,得到麻黄碱盐酸盐。

著录项

  • 公开/公告号IN1997DE00432A

    专利类型

  • 公开/公告日2008-09-12

    原文格式PDF

  • 申请/专利权人

    申请/专利号IN432/DEL/1997

  • 申请日1997-02-21

  • 分类号C07G5/00;

  • 国家 IN

  • 入库时间 2022-08-21 20:07:52

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