首页> 外国专利> TITANIA SOL CHELATED WITH AN ORGANIC COMPLEX, A METHOD THEREOF, AND A COMPOSITION INCLUDING SAID TITANIA SOL FOR FORMING MEDIUM, HIGH, SUPER-HIGH REFRACTIVE INDEX COATING LAYER

TITANIA SOL CHELATED WITH AN ORGANIC COMPLEX, A METHOD THEREOF, AND A COMPOSITION INCLUDING SAID TITANIA SOL FOR FORMING MEDIUM, HIGH, SUPER-HIGH REFRACTIVE INDEX COATING LAYER

机译:用有机配合物螯合的二氧化钛溶胶,其制备方法以及包括所述的二氧化钛溶胶的组合物,用于形成中等,高,超折射指数的涂层

摘要

A method for preparing a titania-organic complex sol as a filler for a composition for forming a medium or higher refraction index coating film is provided to realize excellent compatibility with an organic solvent, shelf stability and monodisperse property, to allow dispersion of a high concentration of titania nanoparticles, and to maintain transparency upon redispersion in an organic solvent. A method for preparing a titania-organic complex sol comprises the steps of: (a) heating a reaction solution containing a titania precursor in a reaction solvent to a sol-gel reaction temperature; (b) adding an acid catalyst to the reaction solution and carrying out a sol-gel reaction to provide a titania sol; (c) adding an organic complex to the titania sol and carrying out a reaction to produce a titania-organic complex sol; (d) drying the reaction solution containing the titania-organic complex sol under an ambient pressure, decreased pressure or freeze-drying condition; and (e) redispersing the dried titania-organic complex in a dispersion solvent.
机译:提供一种制备二氧化钛-有机复合溶胶作为用于形成中等或更高折射率的涂膜的组合物的填料的方法,以实现与有机溶剂的优异相容性,贮存稳定性和单分散性,以允许高浓度分散二氧化钛纳米颗粒,并在重新分散在有机溶剂中时保持透明性。一种制备二氧化钛-有机复合溶胶的方法,包括以下步骤:(a)将在反应溶剂中含有二氧化钛前体的反应溶液加热至溶胶-凝胶反应温度; (b)在反应溶液中加入酸催化剂,并进行溶胶-凝胶反应,得到二氧化钛溶胶。 (c)向二氧化钛溶胶中添加有机配合物,并进行反应以生成二氧化钛-有机配合物溶胶; (d)在环境压力,减压或冷冻干燥条件下干燥含有二氧化钛-有机复合溶胶的反应溶液; (e)将干燥的二氧化钛-有机络合物再分散在分散溶剂中。

著录项

  • 公开/公告号KR20080020848A

    专利类型

  • 公开/公告日2008-03-06

    原文格式PDF

  • 申请/专利权人 LG CHEM. LTD.;

    申请/专利号KR20060084252

  • 发明设计人 IM SANG HYUK;HONG YOUNG JUN;

    申请日2006-09-01

  • 分类号C09D1;C09D5/10;C09D5;

  • 国家 KR

  • 入库时间 2022-08-21 19:54:05

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