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High purity iron and method for producing the same, and high purity iron target

机译:高纯铁及其制造方法以及高纯铁靶

摘要

High purity iron with a very few content of impurities such as copper, a method of manufacturing thereof, and high purity iron targets are provided. The iron containing impurities such as copper is dissolved in a hydrochloric acid solution, and the concentration of the hydrochloric acid of the aqueous solution of iron chloride is adjusted to 0.1 kmol/m3 to 6 kmol/m3. Then, iron is added in the aqueous solution of iron chloride, and an inert gas is injected into the solution with agitating, in order to convert the trivalent iron ions and divalent copper ions contained in the aqueous solution of iron chloride respectively to divalent iron ions and monovalent copper ions. Then, the aqueous solution of iron chloride is fed into a column filled up with the anion exchange resins. The divalent iron ions are not absorbed on the anion exchange resins although the monovalent copper ions are absorbed on the anion exchange resins. Therefore, copper can be separated from the aqueous solution of iron chloride. And then, the aqueous solution of iron chloride is evaporated to dryness, oxidized and heated in a hydrogen atmosphere to generate iron.
机译:提供了具有极少量杂质例如铜的高纯度铁,其制造方法以及高纯度铁靶。将含铜等杂质的铁溶解于盐酸溶液中,将氯化铁水溶液的盐酸浓度调整为0.1kmol / m 3〜6kmol / m 3。然后,将铁添加到氯化铁的水溶液中,并且在搅拌下将惰性气体注入到溶液中,以将氯化铁的水溶液中包含的三价铁离子和二价铜离子分别转化为二价铁离子。和一价铜离子然后,将氯化铁的水溶液进料到装有阴离子交换树脂的塔中。尽管一价铜离子吸收在阴离子交换树脂上,但是二价铁离子没有吸收在阴离子交换树脂上。因此,可以从氯化铁的水溶液中分离出铜。然后,将氯化铁的水溶液蒸发至干,在氢气氛中氧化并加热以产生铁。

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