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Curable butyl rubber PEROXIDE COMPOSITION AND METHOD FOR PRODUCING curable butyl rubber PEROXIDE COMPOSITIONS
Curable butyl rubber PEROXIDE COMPOSITION AND METHOD FOR PRODUCING curable butyl rubber PEROXIDE COMPOSITIONS
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机译:可固化的丁基橡胶过氧化物组合物和制备可固化的丁基橡胶过氧化物组合物的方法
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摘要
1. A process for preparing a peroxide curable composition based on butyl rubber comprising the steps of mixing a non-crosslinked or significantly non-crosslinked (10 wt.% Gel) butyl rubber polymer with a multiolefin (s) crosslinking (s) agent (s), peroxide (s) vulcanizing (s) agent (s) and at least one filler, wherein the method excludes the addition of any non-peroxide vulkanizatorov.2. A method according to claim 1 wherein the butyl polymer comprises the polymerization product of at least one isomonoolefin monomer with 4-7 carbon atoms and at least one multiolefin monomer with 4-14 carbon atoms and, optionally, one or more multiolefin (s) crosslinker (s) agent (s), wherein the multiolefin content (s) agent (s) in the polymer is less than 0.15 mol.%. 3. A method according to claim 1 wherein the multiolefin crosslinking agent is selected from the group consisting of norbornadiene, 2-isopropenyl-norbornene, 5-vinyl-2-norbornene, 1,3,5-hexatriene, 2-phenyl-1,3-butadiene, divinylbenzene, diisopropenylbenzene, divinyltoluene, divinylxylene, substituted alkyl of 1-20 carbon atoms and their derivatives smesi.4. A method according to claim 1, wherein as the peroxide vulcanizer used dialkylperoxides, ketalperoxides, aralkilperoksidy, peroxide ethers and esters efiry.5. A method according to claim 1 wherein the non-crosslinked or significantly non-crosslinked butyl rubber polymer contains less than 5 wt.% Gelya.6. A method according to claim 4, wherein the peroxide vulcanizing agent is selected from the group consisting of di-tret.butilperoksid, bis (t-butylperoxy-isopropyl) -benzene, dicumyl peroxide, 2,5-dimethyl-2,5-di- (tert. butyl-peroxy) -hexane,
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