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REACTION SINTERED ZIRCONIUM CARBIDE/TUNGSTEN COMPOSITE BODIES AND A METHOD FOR PRODUCING THE SAME

机译:反应烧结碳化锆/钨复合体及其制备方法

摘要

A method of sintering a composite body characterized by a transition metal carbide phase (such as a ZrC phase) substantially evenly distributed in a second, typically refractory, transition metal (such as W) matrix at ambient pressures, including blending a first predetermined amount of first transition metal oxide powder (such as ZrO2) with a second predetermined amount of second transition metal carbide powder (such as WC powder). Next the blended powders are mixed to yield a substantially homogeneous powder mixture and a portion of the substantially homogeneous powder mixture is formed into a green body. The body is fired to a first temperature, wherein the first transition metal oxide is substantially reduced and the simultaneously generated CO and gas are evolved from the body to substantially eliminate oxides from the green body, and the body is heated to a second temperature and sintered to yield a composite body of about 99 percent theoretical density and characterized by a first transition metal carbide phase distributed substantially evenly in a second transition metal matrix.
机译:一种烧结复合体的方法,其特征在于过渡金属碳化物相(例如ZrC相)在环境压力下基本均匀地分布在第二个通常为难熔的过渡金属(例如W)基体中,包括混合第一预定量的第一过渡金属氧化物粉末(例如ZrO 2 )和第二预定量的第二过渡金属碳化物粉末(例如WC粉)。接下来,将共混的粉末混合以产生基本上均匀的粉末混合物,并且将一部分基本上均匀的粉末混合物形成生坯。将主体烧成第一温度,其中第一过渡金属氧化物被充分还原,同时产生的一氧化碳和气体从主体中逸出,从而从生坯中基本上消除了氧化物,并且将主体加热到第二温度并烧结。产生约99%理论密度的复合体,其特征在于第一过渡金属碳化物相基本上均匀地分布在第二过渡金属基质中。

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