首页> 外国专利> MANUFACTURING METHOD OF ROD-SHAPED TITANIA NANOPARTICLE CAPABLE OF TRANSFERRING EFFECTIVELY PHOTO CURRENT GENERATED BY DYE OR QUANTUM DOT NANOPARTICLE

MANUFACTURING METHOD OF ROD-SHAPED TITANIA NANOPARTICLE CAPABLE OF TRANSFERRING EFFECTIVELY PHOTO CURRENT GENERATED BY DYE OR QUANTUM DOT NANOPARTICLE

机译:能够转移染料或量子点纳米粒子产生的有效光电流的棒状二氧化钛纳米粒子的制造方法

摘要

PURPOSE: A method for manufacturing a rod-shaped titania nanoparticle for dye or the quantum dot-sensitized solar cell is provided to prepare a rod-shaped titania nanoparticle whose one side is long by using pure titanium tetrachloride without adding a surfactant, etc.;CONSTITUTION: A method for manufacturing a rod-shaped titania nanoparticle comprises the steps of preparing a titanyl chloride (TiOCl2) solution; preparing a dihydroxy oxotitanium (TiO(OH)2) precipitation solution; adding a basic solution to adjust the pH of the dihydroxy oxotitanium precipitation solution to be weak basic, and heating and stirring it; separating dihydroxy oxotitanium from the dihydroxy oxotitanium precipitation solution, and washing it with a weak basic aqueous solution; and adding distilled water and 20 - 500 times of hydrogen peroxide (H2O2) to the washed dihydroxy oxotitanium based on the 1 mol of the Ti^4+ of dihydroxy oxotitanium, and heat treating it to prepare a rod-shaped titania nanoparticle having an average length of 100nm - 300nm.;COPYRIGHT KIPO 2010
机译:用途:提供一种用于染料的棒状二氧化钛纳米粒子或量子点敏化太阳能电池的制造方法,以通过使用纯四氯化钛而不添加表面活性剂等制备一侧长的棒状二氧化钛纳米粒子;等等。构成:一种棒状二氧化钛纳米粒子的制造方法包括以下步骤:制备钛氧基氯(TiOCl2)溶液;制备二羟基氧钛(TiO(OH)2)沉淀溶液;加入碱性溶液调节二羟基氧钛钛沉淀溶液的pH为弱碱性,并加热搅拌。从二羟基氧钛沉淀溶液中分离出二羟基氧钛,并用弱碱性水溶液洗涤;以1摩尔二羟基氧钛的Ti ^ 4 +为基础,向洗涤后的二羟基氧钛中加入蒸馏水和20-500倍的过氧化氢(H2O2),并对其进行热处理,以制备平均分子量为2μm的棒状二氧化钛纳米粒子。长度100nm-300nm。; COPYRIGHT KIPO 2010

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