首页> 外国专利> SIMULTANEOUS ANALYSIS METHOD OF AN AMPHETAMINE DERIVATIVE AND KETAMINE METABOLITE IN HAIR USING GAS CHROMATOGRAPHY

SIMULTANEOUS ANALYSIS METHOD OF AN AMPHETAMINE DERIVATIVE AND KETAMINE METABOLITE IN HAIR USING GAS CHROMATOGRAPHY

机译:气相色谱法同时分析头发中的安非他命衍生物和酮胺代谢物

摘要

PURPOSE: A simultaneous analysis method of an amphetamine derivative and ketamine metabolite is provided to simultaneously analyze total 5 components of amphetamine derivative and ketamine metabolite, and to enable fast analysis through introduction of an automatic cutting process.;CONSTITUTION: A simultaneous analysis method of an amphetamine derivative and ketamine metabolite comprises the steps of: putting a hair sample in a tube containing beads; cutting the sample to a particle size of micrometers using an automatic cutting device at 3000-8000 rpm for 30 seconds-2 minutes; extracting the cut sample with methanol; centrifuging and filtering the extract; and separating the filtrate through heptaflourobutyric acylation derivatization using a HFBA(heptaflourobutyric anhydride) compound.;COPYRIGHT KIPO 2010
机译:目的:提供了一种苯丙胺衍生物和氯胺酮代谢物的同时分析方法,可同时分析苯丙胺衍生物和氯胺酮代谢物的总共5个成分,并通过引入自动切割工艺来进行快速分析。苯丙胺衍生物和氯胺酮代谢物包括以下步骤:将头发样品放入装有小珠的试管中;使用自动切割装置以3000-8000 rpm的速度将样品切割成微米大小的颗粒30秒至2分钟;用甲醇提取切割后的样品;离心和过滤提取物;并通过使用HFBA(七氟丁酸酐)化合物进行七氟丁酸酰化衍生分离滤液。; COPYRIGHT KIPO 2010

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