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Method for preparation of metal organic framework using the sonochemical method and metal organic framework prepared thereby
Method for preparation of metal organic framework using the sonochemical method and metal organic framework prepared thereby
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机译:使用声化学方法制备金属有机骨架的方法和由此制备的金属有机骨架
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摘要
PURPOSE: A method for preparing a metal organic framework using ultrasonic wave is provided to shorten preparation time using quick cooling rate. CONSTITUTION: A method for preparing a metal organic framework(MCF-5) using ultrasonic wave comprises: a step 1 of adding Zn(NO3)26H2O and terephthalic acid to a first solvent to obtain solution; a step 2 of forming a metal organic framework(MOF-5) particle and cooling at room temperature; and a step 3 of collecting washing particles with the first solvent and second solvent and drying. The first or second solvent is each n-methyl-2-pyrrolidone(NMP), N,N-dimethylformamide, chlorobenzene, methanol, ethanol, dimethylacetateamide, acetonitrille, chloroform, tetrahydrofuran or acetone.
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