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METHOD FOR PRODUCING ARBITRALLY BINDED POLYSACCHARIDES

机译:任意键合多糖的制备方法

摘要

1. A method of obtaining a randomly bound polysaccharide containing as ingredients a saccharide, polyol and acid serving as a catalyst, which includes the steps of feeding the ingredients to the reactor to dehydrate the feed ingredients to form anhydrous, mainly syrup, and polycondensate anhydrous, mainly syrup, at elevated temperatures in the specified reactor with simultaneous removal of water generated during the reaction, characterized in that the reactor is a kneading-mixing device with rotating in opposite directions by blades, in which, at the feeding stage, the saccharide, polyol and acid serving as a catalyst are fed into the reactor simultaneously or sequentially, and in which at the stage of dehydration and polycondensation, free water and water generated during the reaction are removed from the indicated device as a result kneading-mixing processing of the supplied ingredients and the resulting anhydrous, mainly syrup, under reduced pressure in the reactor, and during the polycondensation anhydrous, mainly syrup, is continuously mixed vayut in said reactor until the desired degree of polymerization. ! 2. The method according to claim 1, characterized in that the kneading-mixing device is heated to a temperature in the range of 160-220 ° C. ! 3. The method according to claim 2, characterized in that the kneading-mixing device is heated to a temperature in the range 175-200 ° C. ! 4. The method according to claim 3, characterized in that the kneading-mixing device is heated to a temperature in the range 175-190 ° C. ! 5. The method according to any one of the preceding claims 1 to 4, characterized in that the reduced pressure in the kneading and mixing device
机译:1.一种获得含有作为催化剂的糖,多元醇和酸作为成分的无规结合多糖的方法,该方法包括以下步骤:将所述成分进料到反应器中以使进料成分脱水以形成无水(主要是糖浆)和无水缩聚物。 ,主要是糖浆,在指定的反应器中在高温下同时除去反应过程中产生的水,其特征在于该反应器是捏合混合装置,通过叶片沿相反方向旋转,其中在进料阶段,糖类将作为催化剂的多元醇和酸同时或依次加入到反应器中,并且在脱水和缩聚阶段,将游离水和反应过程中产生的水从指示的装置中除去,作为捏合-混合处理的结果。在反应器中减压过程中以及在运行过程中,所提供的成分和所得的无水(主要是糖浆)在所述反应器中将无水的缩水(主要是糖浆)连续混合,直到所需的聚合度。 ! 2.根据权利要求1所述的方法,其特征在于,将所述捏合混合装置加热至160-220℃的温度。 3.根据权利要求2所述的方法,其特征在于,将所述捏合混合装置加热至175-200℃的温度。 4.根据权利要求3所述的方法,其特征在于,将所述捏合混合装置加热至175-190℃的温度。 5.根据前述权利要求1至4中任一项所述的方法,其特征在于,所述捏合和混合装置中的减压

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