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METHOD OF OBTAINING COLLOIDAL SOLUTIONS OF ZINC OXIDE IN NONPOLAR SOLVENTS

机译:在非极性溶剂中获得氧化锌胶体溶液的方法

摘要

1. A process for the preparation of colloidal solutions of zinc oxide in non-polar solvents, comprising heating a reaction mixture of oleylamine, oleic acid and the inorganic zinc-containing precursor in an inert atmosphere, isothermal exposure, the addition of polar solvent, the separation of coagulated nanoparticles centrifugation redispersion precipitate in a nonpolar solvent, wherein in that the zinc-containing precursor using zinc nitrate implementation heating the reaction mixture to 80-100 ° C for 15-30 min and then heated at a temperature of 200-250 ° C for 1-4 hours.! 2. A method according to claim 1, characterized in that the starting reaction mixture was further added diphenyl ether. ! 3. A method according to claim 1, characterized in that the starting reaction mixture was further added hexadecane.
机译:1.制备氧化锌在非极性溶剂中的胶体溶液的方法,包括在惰性气氛中加热油胺,油酸和无机含锌前体的反应混合物,等温暴露,添加极性溶剂,在非极性溶剂中分离凝固的纳米颗粒,离心再分散沉淀,其中使用硝酸锌实施方式的含锌前体将反应混合物加热至80-100°C 15-30分钟,然后在200-250的温度下加热°C 1-4小时。 2.根据权利要求1的方法,其特征在于,进一步将起始反应混合物加入二苯醚。 ! 3.根据权利要求1的方法,其特征在于,进一步将起始反应混合物加入十六烷中。

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