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METHOD OF DETERMINING CONTENT OF LIQUID-PHASE AND SOLID-STATE COMPONENTS IN HYDROCARBON MIXTURE
METHOD OF DETERMINING CONTENT OF LIQUID-PHASE AND SOLID-STATE COMPONENTS IN HYDROCARBON MIXTURE
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机译:测定烃混合物中液相和固相成分含量的方法
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摘要
FIELD: chemistry.;SUBSTANCE: invention can be used to determine content of liquid-phase and solid-state components in a mixture of hydrocarbons. A sample of the hydrocarbon mixture is taken, after which a set of free induction decay curves of the mixture of hydrocarbons is measured using nuclear magnetic resonance for the given sample at temperature ranging from -150°C to +150°C. Content of the solid-state component Ps in the nuclear magnetic resonance 1H signal is determined from each free induction decay curve at the same temperature at which it was measured. From the obtained values, temperature dependence of content of the solid-state component Ps in the nuclear magnetic resonance 1H signal is determined and from the difference Ps - ΔPsi, resulting from phase transition of the i-th component after heating or cooling, content of solid-state and/or liquid-phase components in the mixture of hydrocarbons is determined by assigning ΔPsi values to corresponding components of the mixture.;EFFECT: fast and simple process of determining content of liquid-phase and solid-state components in a mixture of hydrocarbons which avoids complex operations for chemical processing of the mixture.;6 dwg
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机译:领域:化学物质:本发明可用于确定烃混合物中液相和固态组分的含量。采集碳氢化合物混合物的样品,之后,对于给定的样品,在-150°C至+ 150°C的温度范围内,使用核磁共振测量碳氢化合物混合物的一组自由感应衰减曲线。根据在相同温度下的每条自由感应衰变曲线,确定核磁共振 1 Sup> H信号中固态成分P s Sub>的含量。根据获得的值,确定核磁共振 1 Sup> H信号中固态成分P s Sub>的含量与温度的关系,并根据差值P s确定 Sub>-ΔP si Sub>,由加热或冷却后第i个组分的相变产生,烃混合物中固态和/或液相组分的含量由将ΔP si Sub>值分配给混合物的相应组分。效果:快速,简单的确定烃混合物中液相和固态组分含量的过程避免了复杂的化学过程混合物。; 6 dwg
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