Microwave assisted chemical synthesis instrument pressure release is controlled

摘要

For performing microwave-assisted chemical processes that are [SOLUTION] control, particularly useful devices are disclosed for handling the relatively small sample. A microwave transparent reaction vessel having a mouth opened, a pressure resistance seal of the mouth on the container, and includes a needle, the device through the seal at the first end of the needle portion of the needle , I want to form a fluid communication with the vessel. Located at the opposite end of the needle, the pressure transducer is in fluid communication with the interior of the container through the needle. Instrument, has been defining a pressure control fluid flow path to port from the portion of the needle on the outside of the container, the flow path is in fluid communication with the converter and internal needle, of the container. The controllable pressure relief valve of the flow passage, port is incidental.