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Process for extraction of glaucine halogene hydrates from Glaucium flavum

机译:从黄精中提取草甘膦卤水合物的方法

摘要

The invention relates to processes for extraction of biologically active compounds from plant raw material for pharmacological purposes, in particular to a process for extraction of glaucine halogene hydrates from Glaucium flavum.The process, according to the invention, includes shredding of aboveground plant parts, extraction of raw material with water in a ratio of 1:5 at a temperature of 10...100°C and constant stirring for 1...10 hours, filtration of water extract, alkalinization of extract and its extraction with an organic solvent, separation of organic phase, partial distillation of organic solvent in vacuum and treatment of the residual solution with hydrogen chloride or hydrogen bromide with the deposition of salt crystals, their filtration, washing and drying.
机译:本发明涉及用于药理学目的从植物原料中提取生物活性化合物的方法,特别是涉及从黄精中提取青草素卤化物水合物的方法。根据本发明的方法包括将地上植物部分切碎,提取。在10 ... 100°C的温度下以1:5的比例用水与原料混合并持续搅拌1 ... 10小时,过滤水提取物,碱化提取物并用有机溶剂提取,分离有机相,在真空中部分蒸馏有机溶剂,并用氯化氢或溴化氢处理残留溶液,并沉积盐晶体,将其过滤,洗涤和干燥。

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