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PROCESS OF PURIFICATION OF BIO-DIESEL OBTAINED BY THE ESTER INTERCHANGE OF TRIGLYCERIDES IN BASIC CATALYSIS

机译:碱性催化剂中三酯的酯交换纯化生物柴油的工艺

摘要

The invention relates to a process of purification of a bio-diesel fuel. According to the invention, the process comprises the extraction with de-ionized glycerol of the bio-diesel fuel obtained by the ester interchange of triglycerides with lower alcohols in basic catalysis in a glycerol:fuel volumetric ratio of 1:1...1:6, at a temperature of 50...65°C, followed by methanol removal by vaporization at a temperature of 135...140°C and a pressure of 400 torr, for 30 min, the extraction of glycerol and alkalinity traces with demineralized water, the product being then subjected to water evaporation and finally to filtration, thereby resulting a fuel containing in mass percentage 0.25% total glycerol, 0.02% free glycerol, 0.2% methanol and an acid value of 0.5 KOH/g.
机译:本发明涉及一种生物柴油燃料的纯化方法。根据本发明,该方法包括用去离子甘油提取生物柴油燃料,该生物柴油燃料是在碱性催化下甘油酯与燃料的体积比为1:1 ... 1:如图6所示,在50 ... 65°C的温度下,然后在135 ... 140°C的温度和400 torr的压力下汽化除去甲醇,历时30分钟,用二氯甲烷萃取甘油和碱度痕迹。脱矿质水,然后将产物进行水蒸发,最后进行过滤,从而得到一种燃料,其质量百分比为0.25%的总甘油,0.02%的游离甘油,0.2%的甲醇和0.5 KOH / g的酸值。

著录项

  • 公开/公告号RO125428B1

    专利类型

  • 公开/公告日2011-05-30

    原文格式PDF

  • 申请/专利权人 ANDREI MARIAN;

    申请/专利号RO20080000905

  • 发明设计人 ANDREI MARIAN;

    申请日2008-11-20

  • 分类号B01D11/04;C10L1/02;

  • 国家 RO

  • 入库时间 2022-08-21 18:04:46

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