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Manufacturing method of low temperature sintered SiC having superplasticity or high deformation rate

机译:具有超塑性或高变形率的低温烧结SiC的制造方法

摘要

The present invention relates to a method for producing low-temperature sintered silicon carbide exhibiting superplasticity or high-speed deformation, and to silicon carbide prepared as described above, and more specifically, as a sintering aid, Al + B + C, Al + B 4 C + C, Materials obtained by calcining at least one selected from Al 4 C 3 + B + C, or Al 4 C 3 + B 4 C + C at a temperature ranging from 1300 to 1900 ° C., for example Al 8 B 4 C 7 or By synthesizing Al 3 BC 3 and used alone or in combination to sinter the silicon carbide, densified silicon carbide close to the theoretical density can be produced despite sintering at a lower temperature and shorter time than the normal sintering temperature of silicon carbide. It provides a method for producing low-temperature sintered silicon carbide that exhibits superplasticity or high-speed deformation, so that the silicon carbide produced as described above.;According to the present invention, even though silicon carbide is sintered at a lower temperature and shorter time than a conventional sintering temperature, a very densified sintered body can be obtained, and the manufactured silicon carbide has nanoparticles having fine particles of 3 μm or less, preferably 500 nm or less. As a result, it is possible to reduce expensive silicon carbide manufacturing costs, and even in the case of growing the particle size up to 500 nm, it exhibits superplastic behavior at a lower temperature than that of the silicon carbide sintered body manufactured by the conventional method. There is an advantage that can improve the processing performance of the silicon carbide sintered under.;In addition, silicon carbide sintered by hot sintering using low-cost silicon carbide powder in sub-micrometer units also exhibits high-speed deformation behavior at a low temperature of 1600 ° C, further increasing the possibility of practical use. It includes the advantages.;Superplasticity, high speed deformation, silicon carbide, low temperature sintering, sintering aid, Al8B4C7, Al3BC3, calcination, theoretical density
机译:本发明涉及一种生产具有超塑性或高速变形的低温烧结碳化硅的方法,并涉及如上所述制备的碳化硅,更具体地讲,作为烧结助剂,Al + B + C,Al + B 4 C + C,煅烧至少一种选自Al 4 C 3 + B + C或Al 4的材料 C 3 + B 4 C + C在1300至1900°C的温度范围内,例如Al 8 B 4 C 7 或通过合成Al 3 BC 3 单独使用或组合使用来烧结碳化硅,尽管在比正常碳化硅的烧结温度低的温度和较短的时间下烧结,仍可以生产接近理论密度的致密碳化硅。它提供了一种生产具有超塑性或高速变形的低温烧结碳化硅的方法,从而如上所述地生产了碳化硅。根据本发明,即使在较低的温度和较短的温度下烧结碳化硅也是如此。与常规的烧结温度相比,可以得到非常致密的烧结体,并且所制造的碳化硅具有具有3μm以下,优选为500nm以下的微粒的纳米颗粒。结果,可以降低昂贵的碳化硅制造成本,并且即使在将粒径增大到500nm的情况下,其在比常规制造的碳化硅烧结体更低的温度下仍表现出超塑性行为。方法。有一个优点是可以改善在其下烧结的碳化硅的加工性能。此外,以亚微米单位使用低成本碳化硅粉末通过热烧结而烧结的碳化硅在低温下也表现出高速变形行为。 1600℃的温度,进一步增加了实际使用的可能性。它具有以下优点:超塑性,高速变形,碳化硅,低温烧结,烧结助剂,Al8B4C7,Al3BC3,煅烧,理论密度

著录项

  • 公开/公告号KR101072594B1

    专利类型

  • 公开/公告日2011-10-11

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20090037740

  • 申请日2009-04-29

  • 分类号C01B31/36;C04B35/565;B82Y40;

  • 国家 KR

  • 入库时间 2022-08-21 17:49:39

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