首页> 外国专利> METHOD FOR PREPARING ORGANOSILOXANE OLIGOMER COMPOSITION, ORGANOSILOXANE OLIGOMER COMPOSITION, METHOD FOR PRODUCING POLYORGANOSILOXANE CURED FILM, AND POLYORGANOSILOXANE CURED FILM

METHOD FOR PREPARING ORGANOSILOXANE OLIGOMER COMPOSITION, ORGANOSILOXANE OLIGOMER COMPOSITION, METHOD FOR PRODUCING POLYORGANOSILOXANE CURED FILM, AND POLYORGANOSILOXANE CURED FILM

机译:制备有机硅氧烷低聚物组合物的方法,有机硅氧烷低聚物组合物,制备聚有机硅氧烷的薄膜的方法和聚有机硅氧烷的薄膜

摘要

PROBLEM TO BE SOLVED: To provide a method for producing an organosiloxane oligomer which is excellent in storage stability or the like for obtaining a cured film excellent in flaw resistance, crack resistance, adhesion with a base material, or the like.;SOLUTION: The method for preparing an organosiloxane oligomer composition includes: hydrolyzing and condensing organosilane substantially without an ion exchange resin in the presence of water of an amount by mole ratio of 1.0 or more and 5.0 or less relative to a theoretical quantity needed for hydrolysis of the organosiloxane, the water with pH of 5.0 or more and 8.0 or less which is adjusted using a pH adjuster as needed; and thereafter adjusting the pH of the reaction system within the range of 3.0 to 5.5.;COPYRIGHT: (C)2012,JPO&INPIT
机译:解决的问题:提供一种生产具有优异的储存稳定性等的有机硅氧烷低聚物的方法,以获得具有优异的抗裂性,抗裂性,与基材的粘合性等的固化膜。制备有机硅氧烷低聚物组合物的方法包括:在水的存在下,相对于有机硅氧烷水解所需的理论量的摩尔比为1.0以上且5.0以下的量,基本上在没有离子交换树脂的情况下基本上水解和缩合有机硅烷, pH值在5.0以上至8.0以下的水,可根据需要使用pH调节剂进行调节;然后在3.0到5.5的范围内调节反应体系的pH。版权所有:(C)2012,JPO&INPIT

著录项

  • 公开/公告号JP2011246702A

    专利类型

  • 公开/公告日2011-12-08

    原文格式PDF

  • 申请/专利权人 MITSUBISHI RAYON CO LTD;

    申请/专利号JP20110097462

  • 申请日2011-04-25

  • 分类号C08G77/04;B32B27/00;B32B37/00;

  • 国家 JP

  • 入库时间 2022-08-21 17:38:57

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