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FERRULE FOR MAKING FINGERTIGHT COLUMN CONNECTIONS IN GAS CHROMATOGRAPHY

机译:用于在气相色谱中建立手指直柱连接的套圈

摘要

A ferrule arrangement for use in sealing connections to gas chromatography columns includes a generally tubular metal ferrule with an axial bore to receive a fracturable column with a protective coating. The ferrule has a forward part that tapers to a tip region of the ferrule. A generally tubular former has a socket portion to receive the ferrule and further has an internal conical surface that, after such receipt, engages the forward part of the ferrule. A portion is provided on either or both of said ferrule and the former by which the ferrule and former may be directly or indirectly relatively moved together by application of finger force. The taper and the internal conical surface exhibit relative taper angles and the tip region of the ferrule is sufficiently radially thin whereby the application of finger force (i) is adequate to move the ferrule axially into the former to cause the conical surface to engage the tip region of the ferrule and to deform the tip region into sealing engagement with the protective coating of the column, but (ii) does not break the column.
机译:用于与气相色谱柱密封连接的套圈装置包括大体呈管状的金属套圈,该金属套圈具有轴向孔,以容纳具有保护涂层的易碎柱。套圈具有向前部分,该部分逐渐变细到套圈的尖端区域。大体为管状的成形器具有用于容纳套圈的承窝部分,并且还具有内部圆锥形表面,该圆锥形内表面在这种接纳之后与套圈的前部接合。在所述套圈和成形器中的一个或两个上设置有一部分,通过该部分,可以通过施加手指力将套圈和成形器直接或间接地相对地相对移动在一起。锥角和内部圆锥表面具有相对的锥角,并且套圈的尖端区域在径向上足够薄,因此施加手指力(i)足以使套圈轴向移动到前者中,从而使圆锥形表面与尖端接合套圈的区域,并使尖端区域变形,使其与色谱柱的保护层密封接合,但(ii)不会破坏色谱柱。

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