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Process for the Synthesis of Melamine Cyanurate in Lamellar Crystalline Shape with High Purity and Flowability

机译:具有高纯度和流动性的层状晶体形状的三聚氰胺氰尿酸酯的合成方法

摘要

The present invention relates to a process for the synthesis of melamine cyanurate in lamellar crystalline shape with high purity and flowability. The procedures include that 1) melamine and cyanuric acid react to form mixture solution, 2) the mixture solution is filter-pressed to prepare filter cake, 3) filter cake and silicon oil are mixed to obtain semi-finished product, 4) dried the semi-finished product until the water content is less than 1.0%, 5) heat the temperature and control certain vacuum degree for curing and crystallizing, 6) the product is obtained. The processing steps of present invention are easy to operate, the processing parameters are easy to control, the production time of melamine cyanurate is short, the quantity of pure water is low, and utilization of equipments is high. Removing the incompletely reacted raw materials and impurities by filter-pressing, greatly increases the purity of semi-products.
机译:本发明涉及具有高纯度和流动性的层状晶体形状的蜜胺氰尿酸酯的合成方法。程序包括:1)三聚氰胺与氰尿酸反应形成混合溶液,2)将该混合溶液压滤以制备滤饼,3)将滤饼和硅油混合以获得半成品,4)干燥。直到含水量小于1.0%的半成品; 5)加热温度并控制一定的真空度以进行固化和结晶; 6)获得产品。本发明的工艺步骤易于操作,工艺参数易于控制,氰尿酸三聚氰胺的生产时间短,纯水量少,设备利用率高。通过压滤除去未反应的原料和杂质,大大提高了半成品的纯度。

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