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PROCESS FOR PREPARING L-POLYLACTIC ACID BY MICROWAVE-ASSISTED SYNTHESIS

机译:微波辅助合成制备L-聚乳酸的方法

摘要

The invention relates to a process for the synthesis of highly pure L-polylactic acid. According to the invention, the process comprises the solvent free melt-polycondensation of the L enantiomer of the lactic acid at the temperature of 100...130°C, a pressure of 60...80 bar and an irradiation power of 800...1000 W, for 10...30 min, followed by isolating the polylactic acid by dissolving it into dichloromethane and precipitating it with water.
机译:本发明涉及合成高纯度L-聚乳酸的方法。根据本发明,该方法包括在100 ... 130℃的温度,60 ... 80巴的压力和800的照射功率下,乳酸的L对映异构体的无溶剂熔融缩聚。 ..1000 W,持续10 ... 30分钟,然后通过将聚乳酸溶解在二氯甲烷中并用水使其沉淀来分离聚乳酸。

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