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PROCESS FOR PREPARING MAGNETITE OR MAGHEMITE NANOPARTICLES WITH CONTROLLED SIZE USING MILD CONDITIONS

机译:使用轻度条件制备尺寸可控的磁铁矿或镁铁矿纳米颗粒的方法

摘要

The invention relates to an improved process for preparing magnetite or maghemite nanoparticles with controlled size using mild conditions. The process according to the invention comprises coprecipitation of Fe2+ and Fe3+ ions in an aqueous solution under mild alkaline conditions in a pH range from 8 to 12 and a temperature from 15 to 40°C. In a more specific embodiment of the process according to the present invention, the coprecipitation is effected by providing an aqueous reaction medium comprising deionized water set to the desired pH and continuously adding a mixed aqueous solution of Fe2+ and Fe3+ salts to the reaction medium.
机译:本发明涉及在温和条件下制备尺寸可控的磁铁矿或磁赤铁矿纳米颗粒的改进方法。根据本发明的方法包括在pH为8至12的温和碱性条件下,在水溶液中共沉淀Fe 2 + 和Fe 3 + 离子。 15至40°C。在本发明方法的一个更具体的实施方案中,通过提供包含设定为所需pH的去离子水的水性反应介质并连续添加Fe 2 + 的混合水溶液来进行共沉淀。和Fe 3 + 盐加入反应介质中。

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