首页> 外国专利> IODIDE SINGLE CRYSTAL, METHOD FOR PRODUCTION THE IODIDE SINGLE CRYSTAL, AND SCINTILLATOR COMPRISING THE IODIDE SINGLE CRYSTAL

IODIDE SINGLE CRYSTAL, METHOD FOR PRODUCTION THE IODIDE SINGLE CRYSTAL, AND SCINTILLATOR COMPRISING THE IODIDE SINGLE CRYSTAL

机译:碘化物单晶,生产碘化物单晶的方法以及包括碘化物单晶的闪烁器

摘要

An object of the invention is to provide an iodide single crystal material that provides a scintillator material for the next-generation TOF-PET, and a production process for high-quality iodide single crystal materials. The iodide single crystal material of the invention having the same crystal structure as LuI 3 and activated by a luminescence center RE where RE is at least one element selected from the group consisting of Ce, Pr, Nd, Sm, Eu, Tb, Dy, Ho, Er, Tm, and Yb is characterized in that a part or the whole of lutetium (Lu) in said iodide single crystal material is substituted by Y and/or Gd. The inventive production process for an iodide single crystal material is characterized by comprising a step of preparing starting materials comprising an RE metal or PEI 3 , I 2 , and a metal of at least one element selected from the group consisting of Lu, Y and Gd and/or its iodide provided that when only Lu is selected, there is a Lu metal chosen; a step of maintaining said starting materials under vacuum; a step of heating said starting materials at a reaction temperature to create a raw polycrystal material containing at least XI 3 :RE where X is said at least one selected element; and a step of turning said raw polycrystal material into a single crystal.
机译:本发明的目的是提供一种为下一代TOF-PET提供闪烁体材料的碘化物单晶材料,以及高质量碘化物单晶材料的生产方法。本发明的碘化物单晶材料,具有与LuI 3相同的晶体结构,并被发光中心RE激活,其中RE是选自Ce,Pr,Nd,Sm,Eu,Tb,Dy, Ho,Er,Tm和Yb的特征在于,所述碘化物单晶材料中的((Lu)的一部分或全部被Y和/或Gd取代。本发明的碘化物单晶材料的生产方法的特征在于包括制备包含稀土金属或PEI 3,I 2以及选自Lu,Y和Gd的至少一种元素的金属的原材料的步骤。和/或其碘化物,前提是仅选择Lu时,会选择Lu金属;将所述原料保持在真空中的步骤;在反应温度下加热所述原料以产生至少包含XI 3:RE的多晶原料的步骤,其中X是所述至少一种选择的元素;将所述多晶原料制成单晶的步骤。

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