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PROCESS FOR PRODUCING DIFRUCTOSE DIANHYDRIDE III CRYSTALS

机译:制备二葡萄糖二酐III晶体的方法

摘要

2,; DFA III, that is, 1,2 ''; 2,3'' two fructose molecules joined together in the (di -D- fructose furanyl North 1,2 '': The present invention looks deep monohydrate dianhydride III 3 ''dianhydride) a solution containing disaccharides lead is hardly decomposed containing 5 or more, preferably DFA III crystal characterized in that having a pH value of 6 to 8, 5 to 8, more preferably of It provides a method of manufacturing. According to the manufacturing method, DFA III is even in the case where crystallization is performed in the circulation system can be produced on a commercial scale without a decrease in the crystallization rate. In this case, (crude -) if the total fructose content is not more than 5% based on solids in the crystallization mother liquor, the fructose content of 1% or less, the effect is further improved.
机译:2 ;; DFA III,即1,2英寸; 2,3''两个果糖分子在(di -D-果糖呋喃基North 1,2''中结合在一起:本发明看起来较深的一水合物二酐III 3''二酐)含有二糖的溶液很难分解,含有5或更优选地,DFA III晶体的特征在于其pH值为6至8、5至8,更优选地,其提供一种制造方法。根据该制造方法,即使在循环系统中进行结晶化的情况下,也可以不降低结晶化速度而以工业规模生产DFA III。在这种情况下,(粗-)如果总果糖含量基于结晶母液中的固体不大于5%,则果糖含量为1%或更少,则效果进一步提高。

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