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PROCESS FOR MAKING HIGH PURIFIED NICKEL SULFATE FROM NICKEL CONCENTRATES, NICKEL MATTE

机译:从镍精矿,磨砂镍中制取高纯度硫酸镍的方法

摘要

PURPOSE: A manufacturing method of high purity nickel sulfate from nickel concentrate and nickel matte is provided to increase efficiency and profitability of the leaching process. CONSTITUTION: A manufacturing method of high purity nickel sulfate from nickel concentrate and nickel matte comprises the following steps: manufacturing raw slurry by pulverizing and distributing the nickel concentrate or nickel matte(a); primarily leaching nickel source from the raw slurry by using high pressure heating reaction; obtaining nickel sulfate leachate from the nickel source by heat pressuring thereof and collecting insoluble noble metal(c); obtaining nickel sulfate leachate by removing Fe component after adding the nickel sulfate aqueous solution into a heat pressuring reaction bath; adding the nickel sulfate aqueous solution into a multi-stage mixed settler and obtaining nickel sulfate purified liquid through the solvent extraction, solvent scrubbing, and solvent stripping(d); and manufacturing nickel sulfate crystal seed from the nickel sulfate purified liquid and obtaining high purity nickel sulfate by repeating heating and cooling(g). [Reference numerals] (a) Manufacturing raw slurry by pulverizing and distributing the nickel concentrate or nickel matte; (b) Primarily leaching nickel source from the raw slurry by using high pressure heating reaction; (c) Obtaining nickel sulfate leachate from the nickel source by heat pressuring thereof and collecting insoluble noble metal; (d) Obtaining nickel sulfate leachate from the nickel source; (e) Obtaining cobalt sulfate collecting solution; (f) Recycling through transient organic solvent purification; (g) Obtaining high purity hexavalent nickel sulfate by repeating heating
机译:目的:提供一种由镍精矿和磨砂镍制造高纯度硫酸镍的方法,以提高浸出过程的效率和利润率。组成:一种由镍精矿和磨砂镍制成的高纯度硫酸镍的方法包括以下步骤:通过粉碎和分配镍精矿或磨砂镍来制造原料浆。主要通过高压加热反应从原料浆中浸出镍源;通过加热镍从镍源中获得硫酸镍浸出液,并收集不溶性贵金属(c);将硫酸镍水溶液加入热压反应浴后,通过除去Fe成分,得到硫酸镍浸出液。将硫酸镍水溶液加入多级混合沉降器中,通过溶剂萃取,溶剂洗涤和溶剂汽提得到硫酸镍纯化液。用硫酸镍纯化液制造硫酸镍晶种,并通过反复加热和冷却获得高纯度的硫酸镍(g)。 [附图标记](a)通过粉碎并分配镍精矿或磨砂镍来制造原浆; (b)首先通过高压加热反应从原料浆中浸出镍源; (c)通过对镍源进行热压而获得其硫酸镍浸出液,并收集不溶性贵金属; (d)从镍源获取硫酸镍浸出液; (e)获得硫酸钴收集溶液; (f)通过瞬时有机溶剂纯化进行再循环; (g)通过重复加热获得高纯度六价硫酸镍

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