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THE FORMATION METHOD OF FLOWER-LIKE SILVER NANO MATERIAL BY USING PULSED PROTON BEAM

机译:脉冲质子束流形成类似银纳米材料的方法

摘要

invention is a silver salt of an alcohol aqueous solution to the prepared aqueous phase and the proton beam irradiation pulse to the step of is a flower shape including relates to a process for the production of nanomaterials. The silver salt is silver nitrate Here, the acid is perchloric acid, and sulfuric acid is at least one may be a selected from the group consisting of alcohol may be a mixture of polyvinyl alcohol and a secondary or tertiary alcohol, in particular , secondary or tertiary alcohol is an alcohol of a carbon number of 3-10, and preferably from isopropyl alcohol. Polyvinyl alcohol, the mixing ratio of the secondary or tertiary alcohol in a weight ratio of 10: 1 to 1: 1 and the number of days, the concentration of the silver salt to the aqueous solution of alcohol may be from 1 mM to 100 mM Irradiating the proton beam pulses, the peak current is 1 to 20 mA, and a pulse width is 50 to 1 ms, repetition rate of the proton beam is a 0.1 to 60 Hz, 1 MeV to 100 MeV of energy beam having an acceleration can be to examine the proton beam irradiation step for irradiating a number of proton beam pulse may be from 1 to 100 hoeil, by adjusting the number of irradiation of a proton beam pulse irradiating the flower shape is easy to shape of nanomaterials it can be controlled. ;
机译:本发明是一种醇水溶液的银盐对制备的水相的质子束辐照脉冲至花形的步骤,涉及一种制备纳米材料的方法。所述银盐是硝酸银。在此,所述酸是高氯酸,并且硫酸是选自以下的至少一种:醇可以是聚乙烯醇和仲或叔醇的混合物,特别是仲或叔醇。叔醇是碳数为3-10的醇,优选为异丙醇。聚乙烯醇,仲或叔醇的重量比为10:1-1:1:1的混合比例以及银盐相对于醇水溶液的天数可以为1 mM至100 mM照射质子束脉冲,峰值电流为1到20 mA,脉冲宽度为50到1 ms,质子束的重复率为0.1到60 Hz,具有加速力的能量束为1 MeV到100 MeV要检查质子束辐照的步骤,辐照质子束脉冲的次数可能是1到100 hoeil,通过调节质子束脉冲辐照的次数可以辐照花朵形状容易控制的纳米材料的形状。 ;

著录项

  • 公开/公告号KR101193241B1

    专利类型

  • 公开/公告日2012-10-18

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20100043176

  • 发明设计人 김계령;송재희;김영준;

    申请日2010-05-07

  • 分类号B82B3;B01J19/08;

  • 国家 KR

  • 入库时间 2022-08-21 17:07:19

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