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Production methodological null weight average molecular weight Mw of the carbon

机译:碳的生产方法学零重均分子量Mw

摘要

PROBLEM TO BE SOLVED: To provide a method for obtaining a carbon fiber precursor fiber, having a high quality and high definition, being excellent in passing stability in the production process of the carbon fiber, and reducing its production energy, while improving productivity and processability, for wet spinning of a PAN-based carbon fiber precursor fiber.;SOLUTION: In the method for producing the carbon fiber precursor fiber, when dry/wet spinning a spinning solution obtained by dissolving polyacrylonitrile-based polymer having a weight average molecular weight Mw of 100,000-700,000, and a polydispersity Mz/Mw representing Z-average molecular weight Mz to weight average molecular weight Mw of 2.7-6 in a solvent at a concentration of not less than 5 wt.% and less than 30 wt.%, the spinning solution is ejected into a coagulation bath having a coagulation value of 17-40 g under coagulation conditions.;COPYRIGHT: (C)2011,JPO&INPIT
机译:解决的问题:提供一种获得高质量且高清晰度的碳纤维前体纤维的方法,所述碳纤维前体纤维在碳纤维的生产过程中具有优异的通过稳定性,并降低其生产能量,同时提高生产率和可加工性。解决方案:在生产碳纤维前体纤维的方法中,当干/湿纺时,通过溶解重均分子量为Mw的聚丙烯腈基聚合物制得的纺丝溶液在溶剂中的浓度不小于5wt。%且小于30wt。%时,其为100,000-700,000,并且代表在溶剂中的Z-平均分子量Mz相对于重均分子量Mw为2.7-6的多分散度Mz / Mw,纺丝溶液在凝结条件下被喷射到凝结值为17-40 g的凝结浴中。版权所有:(C)2011,JPO&INPIT

著录项

  • 公开/公告号JP5169939B2

    专利类型

  • 公开/公告日2013-03-27

    原文格式PDF

  • 申请/专利权人 東レ株式会社;

    申请/专利号JP20090076110

  • 发明设计人 田中 文彦;野口 知久;川上 大輔;

    申请日2009-03-26

  • 分类号D01F6/18;D01F6/38;D01F9/22;

  • 国家 JP

  • 入库时间 2022-08-21 16:54:48

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