首页>
外国专利>
Method for Separation of Racemic Compound-Forming Chiral Substances by a Cyclic-Crystallization Process and a Crystallization Device
Method for Separation of Racemic Compound-Forming Chiral Substances by a Cyclic-Crystallization Process and a Crystallization Device
展开▼
机译:通过循环结晶法分离形成外消旋化合物的手性物质的方法和结晶装置
展开▼
页面导航
摘要
著录项
相似文献
摘要
The invention concerns a method for separating a racemic compound-forming chiral substance by a cyclic crystallization process which is conducted in at least one first crystallization unit (10) and in at least one second crystallization unit (18), wherein in a first process cycle an enantiomer is crystallized in the first crystallization unit (10) and a racemic compound is crystallized in the second crystallization unit (18), wherein in a second process cycle the enantiomer is crystallized in the second crystallization unit (18) and the racemic compound is crystallized in the first crystallization unit (10), wherein during each process cycle in at least one process sub-step (B→C, F→G) a mother liquor (12) being contained in the first crystallization unit (10) is mutually exchanged with a mother liquor (20) being contained in the second crystallization unit (18). An auto-seeding process sub-step is applied at the beginning of a process cycle.
展开▼