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METHOD OF MANUFACTURING HIGH PURITY RUTHENIUM POWDERS USING WET CHEMICAL REDUCTION METHOD

机译:湿化学还原法制备高纯R粉的方法

摘要

PURPOSE: A high purity ruthenium powder manufacturing method using a liquefied reduction process is provided to manufacture a high purity ruthenium powder from a ruthenium compound such as ruthenium chloride (RuCl3). CONSTITUTION: A high purity ruthenium powder manufacturing method using a liquefied reduction process comprises the following steps. A solution which contains ruthenium and a solution which contains sodium borohydride are prepared (S110). A ruthenium powder is produced by adding the solution which contains the ruthenium compound to the solution which contains sodium borohydride, and then by adding a reducing agent to cause a ruthenium reduction reaction (S120). The produced ruthenium powder is filtered, washed, and dried (S130). The ruthenium compound is selected among ruthenium chloride, ruthenium-oxide, ruthenium carbonyl, and fluorination ruthenium. [Reference numerals] (AA) Start; (BB) End; (S110) Prepare a solution which contains a ruthenium compound and a solution which contains sodium borohydride; (S120) Reducing the solution; (S130) Washing and drying
机译:目的:提供一种使用液化还原工艺的高纯度钌粉制造方法,以从钌化合物(如氯化钌(RuCl3))制造高纯度钌粉。组成:采用液化还原法制备高纯度钌粉的方法包括以下步骤。制备含有钌的溶液和含有硼氢化钠的溶液(S110)。通过将包含钌化合物的溶液添加到包含硼氢化钠的溶液中,然后通过添加还原剂以引起钌还原反应来制备钌粉末(S120)。将产生的钌粉末过滤,洗涤并干燥(S130)。钌化合物选自氯化钌,氧化钌,羰基钌和氟化钌。 [参考数字](AA)开始; (BB)结束; (S110)准备含有钌化合物的溶液和含有硼氢化钠的溶液。 (S120)减少溶液; (S130)洗涤和干燥

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